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混合树脂复合材料和纳米填充树脂复合材料的固化程度、溶解度及唾液吸附之间的关系

Relationship between the degree of conversion, solubility and salivary sorption of a hybrid and a nanofilled resin composite.

作者信息

da Silva Eduardo Moreira, Almeida Giselle Soares, Poskus Laiza Tatiana, Guimarães José Guilherme Antunes

机构信息

Department of Restorative Dentistry, School of Dentistry, Federal Fluminense University, Niterói, Rio de Janeiro, Brazil.

出版信息

J Appl Oral Sci. 2008 Mar-Apr;16(2):161-6. doi: 10.1590/s1678-77572008000200015.

Abstract

This study analyzed the relationship between the degree of conversion (DC), solubility, and salivary sorption of a hybrid (Filtek P 60) and a nanofilled resin composite (Filtek Supreme), and evaluated the influence of the light-activation mode on these properties. Two light-activation modes were used: Conventional (C; 850 mW/cm(2) for 20 s) and Soft-start (SS; 100-1,000 mW/cm(2) for 10 s + 1,000 mW/cm(2) for 10 s). The DC (%) was evaluated by FT-Raman spectroscopy. The solubility and salivary sorption were measured after immersion in artificial saliva for 7 days. Data were analyzed by ANOVA and Student-Newman-Keuls' test and linear regression analysis (a = 0.05). The DC varied from 50.52% (nanofilled composite) to 57.15% (hybrid composite), and was influenced by the light-activation mode: C > SS. The solubility (0.45 microg/mm(3)) and salivary sorption (8.04 microg/mm(3)) of the nanofilled composite were greater than those of the hybrid composite (0.40 microg/mm(3) / 6.87 microg/mm(3)), and were influenced by the light-activation mode: SS > C. Correlation was found between DC and solubility (r = - 0.89, p<0.05), as well as between solubility and salivary sorption (r = 0.95). These findings suggest that nanofilled composites may present higher degradation in the oral environment than hybrid ones. Soft-start light-activation mode may increase the solubility of resin composites.

摘要

本研究分析了一种混合树脂复合材料(Filtek P 60)和一种纳米填充树脂复合材料(Filtek Supreme)的固化程度(DC)、溶解性及唾液吸附之间的关系,并评估了光固化模式对这些性能的影响。使用了两种光固化模式:传统模式(C;850 mW/cm²,持续20秒)和软启动模式(SS;100 - 1000 mW/cm²,持续10秒 + 1000 mW/cm²,持续10秒)。通过傅里叶变换拉曼光谱法评估DC(%)。将材料浸泡在人工唾液中7天后测量其溶解性和唾液吸附。数据采用方差分析、Student - Newman - Keuls检验和线性回归分析(α = 0.05)。DC在50.52%(纳米填充复合材料)至57.15%(混合复合材料)之间变化,并受光固化模式影响:C > SS。纳米填充复合材料的溶解性(0.45 μg/mm³)和唾液吸附(8.04 μg/mm³)大于混合复合材料(0.40 μg/mm³ / 6.87 μg/mm³),且受光固化模式影响:SS > C。发现DC与溶解性之间存在相关性(r = - 0.89,p<0.05),溶解性与唾液吸附之间也存在相关性(r = 0.95)。这些发现表明,纳米填充复合材料在口腔环境中可能比混合复合材料表现出更高的降解性。软启动光固化模式可能会增加树脂复合材料的溶解性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6fb5/4327638/ff22bb2bd1ed/1678-7757-jaos-16-02-0161-gf01.jpg

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