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[小叶棘豆草化学成分的研究]

[Studies on chemical constituents of herbs of Oxytropis microphylla].

作者信息

Peng Cheng, Yang Zhongduo

机构信息

Insititute of Chemical Engineering, Northwest University for Nationalities, Lanzhou 730030, China.

出版信息

Zhongguo Zhong Yao Za Zhi. 2009 Apr;34(8):1007-8.

Abstract

OBJECTIVE

To study the chemical constituents of Oxytropis microphylla.

METHOD

The compounds were isolated and purified by various column chromatographic techniques and their structures were elucidated on the basis of spectral analysis (EI-MS, 1H-NMR, 13C-NMR).

RESULT

Eight compounds were isolated and identified as kaempferol (1), baicalein (2), 5-hydroxy-7, 8, 4'-trimethoxyflavone (3), stigmasterol (4), stigmast-4-en-3beta-ol (5), beta-sitosterol (6), lupenol (7), dehydrocostus lactone (8).

CONCLUSION

All compounds were isolated for the first time from this plant, compounds 2, 3, 5, and 8 were isolated for the first time from this genus.

摘要

目的

研究小叶棘豆的化学成分。

方法

采用多种柱色谱技术对化合物进行分离纯化,并通过光谱分析(EI-MS、1H-NMR、13C-NMR)确定其结构。

结果

分离得到8个化合物,分别鉴定为山柰酚(1)、黄芩素(2)、5-羟基-7,8,4'-三甲氧基黄酮(3)、豆甾醇(4)、豆甾-4-烯-3β-醇(5)、β-谷甾醇(6)、羽扇豆醇(7)、去氢木香内酯(8)。

结论

所有化合物均首次从该植物中分离得到,化合物2、3、5和8为首次从该属植物中分离得到。

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