JMK Instruments Oy(1), Ankkuritie 1, FI-70460 Kuopio, Finland.
ISA Trans. 2010 Jul;49(3):257-63. doi: 10.1016/j.isatra.2010.04.007. Epub 2010 May 11.
The automatic control of grammage (basis weight) in paper and board production is based upon on-line grammage measurement. Furthermore, the automatic control of other quality variables such as moisture, ash content and coat weight, may rely on the grammage measurement. The integrity of Kr-85 based on-line grammage measurement systems was studied, by performing basic calibrations with traceably calibrated plastic reference standards. The calibrations were performed according to the EN ISO/IEC 17025 standard, which is a requirement for calibration laboratories. The observed relative measurement errors were 3.3% in the first time calibrations at the 95% confidence level. With the traceable basic calibration method, however, these errors can be reduced to under 0.5%, thus improving the integrity of on-line grammage measurements. Also a standardised algorithm, based on the experience from the performed calibrations, is proposed to ease the adjustment of the different grammage measurement systems. The calibration technique can basically be applied to all beta-radiation based grammage measurements.
纸张和纸板生产过程中的定量(基重)自动控制基于在线定量测量。此外,其他质量变量(如水分、灰分和涂层重量)的自动控制也可能依赖于定量测量。通过使用可溯源校准的塑料参考标准进行基本校准,研究了基于 Kr-85 的在线定量测量系统的完整性。这些校准是根据 ISO/IEC 17025 标准进行的,这是对校准实验室的要求。在 95%置信水平下,首次校准的观测相对测量误差为 3.3%。然而,通过可溯源的基本校准方法,这些误差可以降低到 0.5%以下,从而提高在线定量测量的完整性。还提出了一种基于所进行校准经验的标准化算法,以简化不同定量测量系统的调整。该校准技术基本上可应用于所有基于β辐射的定量测量。