Nanoscale Res Lett. 2009 Mar 20;4(7):640-5. doi: 10.1007/s11671-009-9295-9.
Cadmium telluride (CdTe) and iron oxide nanoparticles doped silica nanospheres were prepared by a multistep method. Iron oxide nanoparticles were first coated with silica and then modified with amino group. Thereafter, CdTe nanoparticles were assembled on the particle surfaces by their strong interaction with amino group. Finally, an outer silica shell was deposited. The final products were characterized by X-ray powder diffraction, transmission electron microscopy, vibration sample magnetometer, photoluminescence spectra, Fourier transform infrared spectra (FT-IR), and fluorescent microscopy. The characterization results showed that the final nanomaterial possessed a saturation magnetization of about 5.8 emu g(-1) and an emission peak at 588 nm when the excitation wavelength fixed at 380 nm.
碲化镉(CdTe)和氧化铁纳米粒子掺杂二氧化硅纳米球通过多步方法制备。首先,氧化铁纳米粒子被二氧化硅包覆,然后用氨基进行修饰。此后,通过与氨基的强相互作用,CdTe 纳米粒子被组装在颗粒表面上。最后,沉积了一层外二氧化硅壳。通过 X 射线粉末衍射、透射电子显微镜、振动样品磁强计、光致发光光谱、傅里叶变换红外光谱(FT-IR)和荧光显微镜对最终产物进行了表征。表征结果表明,当激发波长固定在 380nm 时,最终的纳米材料具有约 5.8emu g(-1)的饱和磁化强度和 588nm 的发射峰。