Department of Orthodontics, Karadeniz Technical University, Trabzon, Turkey.
Eur J Orthod. 2011 Apr;33(2):174-9. doi: 10.1093/ejo/cjq048. Epub 2010 Jul 21.
The aim of this study was to investigate the effects of surface conditioning protocols on the shear bond strength (SBS) of metal brackets to aged composite resin surfaces in vitro. Ninety composite resin discs, 6 mm in diameter and 2 mm in height, were prepared and treated with an ageing procedure. After ageing, the specimens were randomly assigned to one of the following groups: (1) control with no surface treatment, (2) 38 per cent phosphoric acid gel, (3) 9.6 per cent hydrofluoric acid gel, (4) airborne aluminium trioxide particle abrasion, (5) sodium bicarbonate particle abrasion, and (6) diamond bur. The metal brackets were bonded to composite surfaces by means of an orthodontic adhesive (Transbond XT). All specimens were stored in water for 1 week at 37°C and then thermocycled (1000 cycles, 5-55°C) prior to SBS testing. SBS values and residual adhesive on the composite surface were evaluated. Analysis of variance showed a significant difference (P = 0.000) between the groups. Group 6 had the highest mean SBS (10.61 MPa), followed by group 4 (10.29 MPa). The results of this study suggest that a clinically acceptable bond strength can be achieved by surface conditioning of aged resin composite via the application of hydrofluoric acid, aluminium trioxide particle abrasion, sodium bicarbonate particle abrasion, or a diamond bur.
本研究旨在探讨表面处理方案对体外老化复合树脂表面金属托槽剪切粘结强度(SBS)的影响。制备了 90 个直径为 6 毫米、高度为 2 毫米的复合树脂圆盘,并进行了老化处理。老化后,将试件随机分为以下六组之一:(1)无表面处理的对照组,(2)38%磷酸凝胶,(3)9.6%氢氟酸凝胶,(4)氧化铝喷砂,(5)碳酸氢钠喷砂,(6)金刚石车针。通过正畸胶粘剂(Transbond XT)将金属托槽粘结到复合树脂表面。所有试件均在 37°C 水中储存 1 周,然后进行 SBS 测试前的热循环(1000 次,5-55°C)。评估 SBS 值和复合表面上的残留粘结剂。方差分析显示各组间有显著差异(P = 0.000)。第 6 组的平均 SBS 值最高(10.61 MPa),其次是第 4 组(10.29 MPa)。本研究结果表明,通过应用氢氟酸、氧化铝喷砂、碳酸氢钠喷砂或金刚石车针对老化的树脂复合材料进行表面处理,可以获得临床可接受的粘结强度。