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使用快速读出探测器进行高速晶体检测与表征

High-speed crystal detection and characterization using a fast-readout detector.

作者信息

Aishima Jun, Owen Robin L, Axford Danny, Shepherd Emma, Winter Graeme, Levik Karl, Gibbons Paul, Ashton Alun, Evans Gwyndaf

机构信息

Diamond Light Source, Harwell Science and Innovation Campus, Didcot, England.

出版信息

Acta Crystallogr D Biol Crystallogr. 2010 Sep;66(Pt 9):1032-5. doi: 10.1107/S0907444910028192. Epub 2010 Aug 13.

Abstract

A novel raster-scanning method combining continuous sample translation with the fast readout of a Pilatus P6M detector has been developed on microfocus beamline I24 at Diamond Light Source. This fast grid-scan tool allows the rapid evaluation of large sample volumes without the need to increase the beam size at the sample through changes in beamline hardware. A slow version is available for slow-readout detectors. Examples of grid-scan use in centring optically invisible samples and in detecting and characterizing numerous microcrystals on a mesh-like holder illustrate the most common applications of the grid scan now in routine use on I24.

摘要

在钻石光源的微聚焦光束线I24上,开发了一种将连续样品平移与Pilatus P6M探测器的快速读出相结合的新型光栅扫描方法。这种快速网格扫描工具能够快速评估大体积样品,而无需通过改变光束线硬件来增大样品处的光束尺寸。还有一个慢速版本适用于读出速度较慢的探测器。在对光学不可见样品进行对中以及在检测和表征网格状支架上的大量微晶时使用网格扫描的示例,说明了目前I24上常规使用的网格扫描的最常见应用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/72e9/6691516/ef522b52d15c/d-66-01032-fig1.jpg

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