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人工老化对密封复合材料粗糙度和显微硬度的影响。

Effect of artificial aging on the roughness and microhardness of sealed composites.

机构信息

Department of Restorative Dentistry, Araçatuba School of Dentistry, UNESP, Araçatuba, São Paulo, Brazil.

出版信息

J Esthet Restor Dent. 2010 Oct;22(5):324-30. doi: 10.1111/j.1708-8240.2010.00360.x.

Abstract

STATEMENT OF THE PROBLEM

The application of surface sealant could improve the surface quality and success of composite restorations; however, it is important to assess the behavior of this material when subjected to aging procedures.

PURPOSE

To evaluate the effect of artificial aging on the surface roughness and microhardness of sealed microhybrids and nanofilled composites.

MATERIALS AND METHODS

One hundred disc-shaped specimens were made for each composite. After 24 hours, all samples were polished and surface sealant was applied to 50 specimens of each composite. Surface roughness (Ra) was determined with a profilometer and Knoop microhardness was assessed with a 50-g load for 15 seconds. Ten specimens of each group were aged during 252 hours in a UV-accelerated aging chamber or immersed for 28 days in cola soft drink, orange juice, red wine staining solutions, or distilled water. Data were analyzed by two-way analysis of variance and Fischer's test (α=0.05).

RESULTS

Artificial aging decreased microhardness values for all materials, with the exceptions of Vit-l-escence (Ultradent Products Inc., South Jordan UT, USA) and Supreme XT (3M ESPE, St. Paul, MN, USA) sealed composites; surface roughness values were not altered. Water storage had less effect on microhardness, compared with the other aging processes. The sealed materials presented lower roughness and microhardness values, when compared with unsealed composites.

CONCLUSIONS

Aging methods decreased the microhardness values of a number of composites, with the exception of some sealed composites, but did not alter the surface roughness of the materials.

CLINICAL SIGNIFICANCE

The long-term maintenance of the surface quality of materials is fundamental to improving the longevity of esthetic restorations. In this manner, the use of surface sealants could be an important step in the restorative procedure using resin-based materials.

摘要

问题陈述

表面密封剂的应用可以提高复合修复体的表面质量和成功率;然而,评估这种材料在老化程序下的行为是很重要的。

目的

评估人工老化对密封微混合体和纳米填充复合材料表面粗糙度和显微硬度的影响。

材料和方法

每种复合材料制作 100 个圆盘形试件。24 小时后,所有样品均进行抛光,然后在每种复合材料的 50 个试件上施加表面密封剂。使用轮廓仪测定表面粗糙度(Ra),用 50g 负载 15 秒评估克努普显微硬度。每组的 10 个试件在 UV 加速老化箱中老化 252 小时,或在可乐软饮料、橙汁、红酒染色溶液或蒸馏水中共浸泡 28 天。使用双向方差分析和 Fischer 检验(α=0.05)分析数据。

结果

人工老化降低了所有材料的显微硬度值,除了 Vit-l-escence(美国南约旦市 Ultradent Products Inc.)和 Supreme XT(3M ESPE,明尼苏达州圣保罗市)密封复合材料;表面粗糙度值没有改变。与其他老化过程相比,水储存对显微硬度的影响较小。与未密封复合材料相比,密封材料的表面粗糙度和显微硬度值较低。

结论

老化方法降低了许多复合材料的显微硬度值,除了一些密封复合材料外,但没有改变材料的表面粗糙度。

临床意义

长期保持材料表面质量对于提高美学修复体的寿命至关重要。因此,使用表面密封剂可能是使用树脂基材料进行修复程序的重要步骤。

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