Colombo Marco, Gallo Simone, Poggio Claudio, Ricaldone Vittorio, Arciola Carla Renata, Scribante Andrea
Department of Clinical, Surgical, Diagnostic and Paediatric Sciences - Section of Dentistry, University of Pavia, Piazzale Golgi 2, 27100 Pavia, Italy.
IRCCS Istituto Ortopedico Rizzoli, Laboratorio di Patologia delle Infezioni Associate all'Impianto, via di Barbiano 1/10, 40136 Bologna, Italy.
Materials (Basel). 2020 Mar 13;13(6):1308. doi: 10.3390/ma13061308.
The current study evaluated the Vickers hardness number (VHN) and hardness ratio of four bulk-fill composites (VisCalor bulk; Admira Fusion x-tra; x-tra fil; and GrandioSO x-tra-Voco, Cuxhaven, Germany) to assess the risk of bacterial colonization in comparison with standard composite materials. Thirty samples were prepared for each group. The VHN of both the external (top) and internal surface (bottom) was determined with a micro-hardness tester (200 g load for 15 s), and the hardness ratio was also calculated for each sample. Subsequently, storage in an acidic soft drink (Coca-Cola, Coca-Cola Company, Milano, Italy) was performed; for each group, 10 samples were stored for 1 day, while another 10 were stored for 7 days and the remaining 10 were kept in water as controls. A significant reduction in VHN was shown for all the groups when comparing the external versus internal side (P < 0.05), although the hardness ratio was greater than 0.80, resulting in an adequate polymerization. Regarding the acid storage, all the groups showed a significant decrease of VHN when compared with the controls, both after 1 day (P < 0.05) and after 7 days (P < 0.001). All the products showed adequate depth of cure without further risk of bacterial colonization. However, acid exposure negatively affected micro-hardness values, which might promote subsequent colonization.
本研究评估了四种大块充填复合材料(VisCalor bulk;Admira Fusion x-tra;x-tra fil;以及GrandioSO x-tra - Voco,德国库克斯港)的维氏硬度值(VHN)和硬度比,以与标准复合材料相比评估细菌定植风险。每组制备30个样本。使用显微硬度测试仪(200 g载荷,持续15秒)测定外部(顶部)和内部表面(底部)的VHN,并计算每个样本的硬度比。随后,将样本储存在酸性软饮料(可口可乐,可口可乐公司,意大利米兰)中;每组中,10个样本储存1天,另外10个储存7天,其余10个作为对照保存在水中。比较外部和内部时,所有组的VHN均显著降低(P < 0.05),尽管硬度比大于0.80,表明聚合充分。关于酸储存,与对照组相比,所有组在储存1天(P < 0.05)和7天(P < 0.001)后VHN均显著降低。所有产品均显示出足够的固化深度,无进一步细菌定植风险。然而,酸暴露对显微硬度值有负面影响,这可能会促进后续定植。