2,3-二氯-5,6-二氰基对苯醌促进硫代酰胺形成硫硫键的合成。
Synthesis of sulfur-sulfur bond formation from thioamides promoted by 2,3-dichloro-5,6-dicyanobenzoquinone.
机构信息
Department of Medicinal and Applied Chemistry, Kaohsiung Medical University, Kaohsiung City 807, Taiwan.
出版信息
Org Lett. 2010 Dec 3;12(23):5570-2. doi: 10.1021/ol102455x. Epub 2010 Nov 10.
PMID:21067153
Abstract
A mild and efficient synthesis of sulfur-sulfur bond formation from thioformanilides with 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ) is described. Functionality on the aromatic ring plays a key role in the formation of a sulfur-sulfur bond.
摘要
本文描述了一种温和高效的从硫代甲酰胺与 2,3-二氯-5,6-二氰基对苯醌（DDQ）合成硫硫键的方法。芳环上的官能团在硫硫键的形成中起着关键作用。
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