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[细辛挥发油化学成分的气相色谱-质谱联用分析]

[Analysis of the chemical constituents of volatile oil from Asarum insigne by GC-MS].

作者信息

Qu Wan-you, Tan Zhi-Wei, Yu Ai-Nong, Quan Jia-Peng

机构信息

School of Chemical and Environmental Engineering, Hubei Institute for nationalities, Enshi 445000, China.

出版信息

Zhong Yao Cai. 2010 Jul;33(7):1095-8.

Abstract

OBJECTIVE

To analyse the chemical constituents of volatile oil from Asarum insigne.

METHODS

The volatile oil from Asarum insigne was isolated with steam distillation and identified by capillary GC/MS method.

RESULTS

68 Volatile components were identified and determined, accounting for 92.18% of the total peak area. The main volatile compounds and their relative contents are camphene (13.48%), alpha-pinene (12.44%), beta-pinene (11.07%), borneol (8.12%), trans-beta-farnesene (5.91%), elemicin (5.38%), 1,3-benzodioxole-5-(2-propenyl) (3.06%), myristicin (2.95%), ledene (2.47%), eucalyptol (2.33%), patchouli alcohol (2.25%), alpha-bisabolene (2.04%) and bornyl acetate (1.36%) etc.

CONCLUSION

The study provided solid and scientific proof for the exploitation and utilization of Asarum insigne.

摘要

目的

分析单叶细辛挥发油的化学成分。

方法

采用水蒸气蒸馏法提取单叶细辛挥发油,并用毛细管GC/MS法进行鉴定。

结果

鉴定并测定了68种挥发性成分,占总峰面积的92.18%。主要挥发性化合物及其相对含量为莰烯(13.48%)、α-蒎烯(12.44%)、β-蒎烯(11.07%)、冰片(8.12%)、反式-β-金合欢烯(5.91%)、榄香素(5.38%)、1,3-苯并二恶唑-5-(2-丙烯基)(3.06%)、肉豆蔻醚(2.95%)、喇叭烯(2.47%)、桉叶油素(2.33%)、广藿香醇(2.25%)、α-红没药烯(2.04%)和乙酸龙脑酯(1.36%)等。

结论

该研究为单叶细辛的开发利用提供了坚实的科学依据。

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