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成核剂对颌面硅橡胶弹性体尺寸稳定性和细节再现性的影响。

Influence of opacifiers on dimensional stability and detail reproduction of maxillofacial silicone elastomer.

机构信息

Department of Dental Materials and Prosthodontics, Araçatuba Dental School, UNESP, Rua José Bonifácio 1193, Araçatuba, SP, Brazil.

出版信息

Biomed Eng Online. 2010 Dec 16;9:85. doi: 10.1186/1475-925X-9-85.

Abstract

BACKGROUND

We evaluated the influence of chemical disinfection and accelerated aging on the dimensional stability and detail reproduction of a silicone elastomer containing one of two opacifiers.

METHODS

A total of 90 samples were fabricated from Silastic MDX 4-4210 silicone and divided into groups (n = 10) according to opacifier content (barium sulfate or titanium dioxide) and disinfectant solution (neutral soap, Efferdent, or 4% chlorhexidine). The specimens were disinfected 3 times per week during 60 days and then subjected to accelerated aging for 1008 hours. Dimensional stability and detail reproduction tests were performed after specimens' fabrication (baseline), chemical disinfection and periodically during accelerated aging (252, 504, and 1008 hours). The results were analyzed using 3-way repeated-measures ANOVA and the Tukey HSD test (α = 0.05).

RESULTS

All groups exhibited dimensional changes over time. The opacifier (p = .314), period (p < .0001) and their interactions (p = .0041) affected the dimensional stability of the silicone. Statistical significant dimensional differences occurred between groups with (0.071) and without opacifiers (0.053). Accelerated aging influenced the dimensional stability of the samples. All groups scored 2 in the detail reproduction tests, which represents the fully reproducing of three test grooves with accurate angles.

CONCLUSIONS

Incorporation of opacifiers alters the dimensional stability of silicones used in facial prosthetics, but seems to have no influence on detail reproduction. Accelerated aging is responsible for most of the dimensional changes in Silastic MDX4 4210, but all dimensional changes measured in this study remained within the limits of stability necessary for this application.

摘要

背景

我们评估了化学消毒和加速老化对含有两种遮光剂之一的硅橡胶的尺寸稳定性和细节再现的影响。

方法

总共制作了 90 个 Silastic MDX 4-4210 硅橡胶样本,并根据遮光剂含量(硫酸钡或二氧化钛)和消毒剂溶液(中性肥皂、Efferdent 或 4%洗必泰)将其分为 10 组(n = 10)。在 60 天内每周对样本进行 3 次消毒,然后进行 1008 小时的加速老化。在样本制作后(基线)、化学消毒期间以及加速老化期间定期(252、504 和 1008 小时)进行尺寸稳定性和细节再现测试。使用 3 向重复测量方差分析和 Tukey HSD 检验(α = 0.05)分析结果。

结果

所有组在一段时间后都表现出尺寸变化。遮光剂(p =.314)、时间(p <.0001)及其相互作用(p =.0041)影响硅橡胶的尺寸稳定性。有(0.071)和无遮光剂的组之间存在统计学显著的尺寸差异(0.053)。加速老化影响样本的尺寸稳定性。所有组在细节再现测试中得分为 2,这代表准确角度的三个测试槽完全再现。

结论

遮光剂的加入会改变用于面部修复体的硅橡胶的尺寸稳定性,但似乎对细节再现没有影响。加速老化是 Silastic MDX4 4210 尺寸变化的主要原因,但本研究中测量的所有尺寸变化都在该应用所需的稳定性限制内。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9f1b/3224922/6093bf290f6d/1475-925X-9-85-3.jpg

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