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(1R,4R,5R)-1,3,4-Triphenyl-7-[(R)-1-phenyl-ethyl]-2-oxa-3,7-diaza-spiro-[4.5]decan-10-one.

作者信息

Malathy A, Kumar R Suresh, Perumal S, Suresh J, Lakshman Nilantha

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2007 Dec 21;64(Pt 1):o343. doi: 10.1107/S1600536807067256.

DOI:10.1107/S1600536807067256
PMID:21200905
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2915384/
Abstract

In the title compound, C(33)H(32)N(2)O(2), the polysubstituted piperidine ring adopts a chair conformation. The isoxazolidine ring is in an envelope conformation. In the crystal structure, intra- and inter-molecular C-H⋯π inter-actions involving the phenyl rings are observed.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c542/2915384/181814add915/e-64-0o343-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c542/2915384/181814add915/e-64-0o343-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c542/2915384/181814add915/e-64-0o343-fig1.jpg

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本文引用的文献

1
Regio- and stereoselectivity of captodative olefins in 1,3-dipolar cycloadditions. A DFT/HSAB theory rationale for the observed regiochemistry of nitrones.1,3-偶极环加成反应中俘精酸酐烯烃的区域和立体选择性。关于硝酮观察到的区域化学的密度泛函理论/软硬酸碱理论原理。
J Org Chem. 2001 Feb 23;66(4):1252-63. doi: 10.1021/jo001393n.
2
Stereoselective 1,3-dipolar cycloadditions of a chiral nitrone derived from erythrulose. An experimental and DFT theoretical study.由赤藓酮糖衍生的手性硝酮的立体选择性1,3-偶极环加成反应。一项实验与密度泛函理论研究。
J Org Chem. 2000 Oct 20;65(21):7000-9. doi: 10.1021/jo0009651.