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4-氯-N'-(2-羟基-亚苄基)苯甲酰肼一水合物

4-Chloro-N'-(2-hydroxy-benzyl-idene)benzohydrazide monohydrate.

作者信息

Lu Jiu-Fu, Min Suo-Tian, Ji Xiao-Hui, Dang Zhong-Hai

机构信息

School of Chemistry and Environmental Science, Shaanxi University of Technology, Hanzhong 723000, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 6;64(Pt 9):o1694. doi: 10.1107/S1600536808024471.

DOI:10.1107/S1600536808024471
PMID:21201683
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2960496/
Abstract

The asymmetric unit of the title compound, C(14)H(11)ClN(2)O(2)·H(2)O, contains a Schiff base mol-ecule and a water mol-ecule of crystallization. The dihedral angle between the two aromatic rings is 27.3 (4)°. In the crystal structure, mol-ecules are linked into a two-dimensional network parallel to the bc plane by inter-molecular O-H⋯O and N-H⋯O hydrogen bonds involving the water mol-ecules.

摘要

标题化合物C(14)H(11)ClN(2)O(2)·H(2)O的不对称单元包含一个席夫碱分子和一个结晶水分子。两个芳环之间的二面角为27.3 (4)°。在晶体结构中，分子通过涉及水分子的分子间O-H⋯O和N-H⋯O氢键连接成平行于bc平面的二维网络。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5f02/2960496/7ae995f2a2be/e-64-o1694-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5f02/2960496/a5df82e64249/e-64-o1694-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5f02/2960496/7ae995f2a2be/e-64-o1694-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5f02/2960496/a5df82e64249/e-64-o1694-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5f02/2960496/7ae995f2a2be/e-64-o1694-fig2.jpg

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