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N'-[1-(2-羟基苯基)亚乙基]-2-甲氧基苯甲酰肼

N'-[1-(2-Hy-droxy-phen-yl)ethyl-idene]-2-meth-oxy-benzohydrazide.

作者信息

Yue Si-Yu, Lu Jiu-Fu

机构信息

School of Chemistry and Environmental Science, Shaanxi University of Technology, Hanzhong 723000, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 5;66(Pt 7):o1550. doi: 10.1107/S1600536810020477.

DOI:10.1107/S1600536810020477
PMID:21587795
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3006911/
Abstract

There are two independent mol-ecules in the asymmetric unit of the title compound, C(16)H(16)N(2)O(3), in which the dihedral angles between the two aromatic rings are 13.0 (3) and 6.4 (3)°. Intra-molecular O-H⋯N and N-H⋯O hydrogen bonds are observed in both mol-ecules, forming S(6) rings in all cases.

摘要

标题化合物C(16)H(16)N(2)O(3)的不对称单元中有两个独立分子，其中两个芳环之间的二面角分别为13.0 (3)°和6.4 (3)°。在两个分子中均观察到分子内O-H⋯N和N-H⋯O氢键，在所有情况下均形成S(6)环。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0922/3006911/2d60e8c959c9/e-66-o1550-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0922/3006911/2d60e8c959c9/e-66-o1550-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0922/3006911/2d60e8c959c9/e-66-o1550-fig1.jpg

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本文引用的文献

1
N'-[1-(2-Hydroxy-phen-yl)ethyl-idene]-2-nitro-benzohydrazide methanol solvate.N'-[1-(2-羟基苯基)亚乙基]-2-硝基苯甲酰肼甲醇溶剂化物
Acta Crystallogr Sect E Struct Rep Online. 2009 Feb 25;65(Pt 3):o585. doi: 10.1107/S160053680900508X.
2
2-Meth-oxy-N'-(2-methoxy-benzyl-idene)benzohydrazide.2-甲氧基-N'-(2-甲氧基亚苄基)苯甲酰肼
Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 6;64(Pt 9):o1695. doi: 10.1107/S160053680802521X.
3
4-Chloro-N'-(2-hydroxy-benzyl-idene)benzohydrazide monohydrate.4-氯-N'-(2-羟基-亚苄基)苯甲酰肼一水合物
Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 6;64(Pt 9):o1694. doi: 10.1107/S1600536808024471.
4
N'-(2-Hydroxy-benzyl-idene)-2-methoxy-benzohydrazide monohydrate.N'-(2-羟基-亚苄基)-2-甲氧基苯甲酰肼一水合物
Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 6;64(Pt 9):o1693. doi: 10.1107/S1600536808024483.
5
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.