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4-羟基-N'-(4-甲氧基亚苄基)苯甲酰肼

4-Hydr-oxy-N'-(4-methoxy-benzyl-idene)benzohydrazide.

作者信息

Shi Da-Hua

机构信息

School of Chemical Engineering, Huaihai Institute of Technology, Lianyungang Jiangsu 222005, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Aug 8;65(Pt 9):o2107. doi: 10.1107/S1600536809030621.

DOI:10.1107/S1600536809030621
PMID:21577522
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2970054/
Abstract

The title compound, C(15)H(14)N(2)O(3), was synthesized by the reaction of 4-methoxy-benzaldehyde with 4-hydroxy-benzohydrazide in methanol. The mol-ecule adopts an E configuration about the C=N bond. The two benzene rings make a dihedral angle of 46.6 (2)°. In the crystal structure, mol-ecules are linked into a two-dimensional network parallel to (001) through O-H⋯O and N-H⋯O hydrogen bonds.

摘要

标题化合物C(15)H(14)N(2)O(3)是通过4-甲氧基苯甲醛与4-羟基苯甲酰肼在甲醇中反应合成的。分子围绕C=N键采取E构型。两个苯环形成的二面角为46.6 (2)°。在晶体结构中，分子通过O-H⋯O和N-H⋯O氢键连接成平行于(001)的二维网络。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5378/2970054/14ee50b9bdc6/e-65-o2107-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5378/2970054/a158a5e07a42/e-65-o2107-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5378/2970054/14ee50b9bdc6/e-65-o2107-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5378/2970054/a158a5e07a42/e-65-o2107-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5378/2970054/14ee50b9bdc6/e-65-o2107-fig2.jpg

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