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Poly[diaqua-(μ(4)-2,5-dicarb-oxy-benzene-1,4-dicarboxyl-ato-κ(4)O(1):O(2):O(4):O(5))(μ(2)-2,5-dicarb-oxy-benzene-1,4-dicarboxyl-ato-κ(2)O(1):O(4))bis-(1,10-phenanthroline-κ(2)N,N')dimanganese(II)].聚[二水合-(μ(4)-2,5-二羧基苯-1,4-二羧酸根合-κ(4)O(1):O(2):O(4):O(5))(μ(2)-2,5-二羧基苯-1,4-二羧酸根合-κ(2)O(1):O(4))双-(1,10-菲咯啉-κ(2)N,N')二锰(II)]
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本文引用的文献

1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
Diversity in magnetic properties of 3D isomorphous networks of Co(II) and Mn(II) constructed by napthalene-1,4-dicarboxylate.由萘-1,4-二羧酸构建的钴（II）和锰（II）的三维同构网络的磁性多样性。
Chem Commun (Camb). 2005 Sep 28(36):4613-5. doi: 10.1039/b507953e. Epub 2005 Aug 19.

聚[（μ(6)-萘-1,4-二羧酸根合-κO:O:O:O:O:O）铁（II）]

Poly[(μ(6)-naphthalene-1,4-dicarboxyl-ato-κO:O:O:O:O:O)iron(II)].

作者信息

Boeckmann Jan, Jess Inke, Näther Christian

机构信息

Institut für Anorganische Chemie, Christian-Albrechts-Universität Kiel, Max-Eyth Strasse 2, D-24098 Kiel, Germany.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 20;65(Pt 1):m102. doi: 10.1107/S1600536808042669.

DOI:10.1107/S1600536808042669
PMID:21581469
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2968007/
Abstract

In the title compound, Fe(C(12)H(6)O(4)), the Fe(II) atom is coordinated by six O atoms from six symmetrically equivalent naphthalene-1,4-dicarboxyl-ate ligands in a strongly distorted octa-hedral geometry. These octa-hedra are connected via common edges into chains that elongate along the a axis, with Fe⋯Fe distances of 2.9712 (4) and 2.9724 (4) Å. The chains are linked via the naphthalene-1,4-dicarboxyl-ate ligands into a three-dimensional coordination network.

摘要

在标题化合物[Fe(C₁₂H₆O₄)]ₙ中，Fe(II)原子由来自六个对称等效的萘-1,4-二羧酸酯配体的六个O原子配位，形成严重扭曲的八面体几何构型。这些八面体通过共用边连接成沿a轴延伸的链，Fe⋯Fe距离为2.9712 (4)和2.9724 (4) Å。这些链通过萘-1,4-二羧酸酯配体连接成三维配位网络。