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N-（2-羟乙基）-2-[3-（对甲苯基）三氮烯-1-基]苯甲酰胺

N-(2-Hydroxy-ethyl)-2-[3-(p-tol-yl)triazen-1-yl]benzamide.

作者信息

Rocha-Alonzo Fernando, Aguirre Gerardo, Parra-Hake Miguel

机构信息

Centro de Graduados e Investigación del Instituto Tecnológico de Tijuana, Apdo. Postal 1166, 22500, Tijuana, BC, Mexico.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Apr 8;65(Pt 5):o990-1. doi: 10.1107/S1600536809011908.

DOI:10.1107/S1600536809011908
PMID:21584027
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977684/
Abstract

In the solid state, the structure of the title compound, C(16)H(18)N(4)O(2), is stabilized by inter-molecular N-H⋯O and O-H⋯O hydrogen bonds. These hydrogen bonds arrange the mol-ecules into a double-layer supra-molecular structure. The mol-ecular conformation is is consolidated by an intra-molecular N-H⋯N hydrogen bond. The dihedral angle between the aromatic rings is 8.01 (10)°

摘要

在固态下，标题化合物C(16)H(18)N(4)O(2)的结构通过分子间的N-H⋯O和O-H⋯O氢键得以稳定。这些氢键将分子排列成双层超分子结构。分子构象通过分子内的N-H⋯N氢键得以巩固。芳香环之间的二面角为8.01 (10)°

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51f5/2977684/18279b70b21e/e-65-0o990-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51f5/2977684/f443acf191f2/e-65-0o990-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51f5/2977684/acea20c3a886/e-65-0o990-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51f5/2977684/18279b70b21e/e-65-0o990-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51f5/2977684/f443acf191f2/e-65-0o990-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51f5/2977684/acea20c3a886/e-65-0o990-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51f5/2977684/18279b70b21e/e-65-0o990-fig3.jpg

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