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[2,6-Bis(6-methyl-quinolin-2-yl)pyridine-κN,N',N'']dichloridomanganese(II).

作者信息

Li Xiao-Ping, Zhao Jian-She, Ng Seik Weng

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 25;66(Pt 10):m1298. doi: 10.1107/S1600536810037037.

DOI:10.1107/S1600536810037037
PMID:21587437
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2983179/
Abstract

In the mol-ecule of the title compound, [MnCl(2)(C(25)H(19)N(3))], the three N atoms span the axial-equatorial-axial sites of the trigonal-bipyramidal coordination polyhedron; the geometry of the Mn(II) atom is 34% distorted from trigonal-bipyramidal (towards square-pyramidal along the Berry pseudorotation pathway). One of the Cl atoms is disordered over two positions in a 0.82 (3):0.18 (3) ratio. Weak inter-molecular C-H⋯Cl hydrogen bonding occurs in the crystal structure.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2c6a/2983179/52328fe1d2d9/e-66-m1298-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2c6a/2983179/52328fe1d2d9/e-66-m1298-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2c6a/2983179/52328fe1d2d9/e-66-m1298-fig1.jpg

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本文引用的文献

1
{2,6-Bis[(4-bromo-phen-yl)imino-meth-yl]pyridine-κN,N',N''}trichlorido-chromium(III).{2,6-双[(4-溴苯基)亚氨基甲基]吡啶-κN,N',N''}三氯化铬(III)
Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 8;66(Pt 10):m1215. doi: 10.1107/S1600536810034689.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.