Khun N W, Liu E
School of Mechanical and Aerospace Engineering, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore.
J Nanosci Nanotechnol. 2011 Jun;11(6):5292-8. doi: 10.1166/jnn.2011.3769.
Nitrogen doped diamond-like carbon (DLC:N) thin films were deposited on highly conductive p-Si substrates using a DC magnetron sputtering deposition system. The DLC:N films were characterized using X-ray photoelectron spectroscopy (XPS), micro-Raman spectroscopy, atomic force microscopy (AFM), contact angle measurement and micro-scratch test. The XPS and Raman results indicated that the sputtering power significantly influenced the properties of the films in terms of bonding configuration in the films. The corrosion performance of the DLC:N films was investigated in a 0.6 M NaCl solution by means of potentiodynamic polarization testing. It was found that the corrosion performance of the films could be enhanced by higher sputtering powers.
使用直流磁控溅射沉积系统在高导电性p型硅衬底上沉积了氮掺杂类金刚石碳(DLC:N)薄膜。采用X射线光电子能谱(XPS)、显微拉曼光谱、原子力显微镜(AFM)、接触角测量和微划痕试验对DLC:N薄膜进行了表征。XPS和拉曼结果表明,溅射功率在薄膜的键合结构方面对薄膜性能有显著影响。通过动电位极化测试研究了DLC:N薄膜在0.6 M NaCl溶液中的腐蚀性能。结果发现,较高的溅射功率可以提高薄膜的腐蚀性能。