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无任何还原剂的银/壳聚糖/聚乙二醇纳米复合材料的绿色合成与表征

Green synthesis and characterization of silver/chitosan/polyethylene glycol nanocomposites without any reducing agent.

作者信息

Ahmad Mansor Bin, Tay Mei Yen, Shameli Kamyar, Hussein Mohd Zobir, Lim Jenn Jye

机构信息

Department of Chemistry, Faculty of Science, Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, Malaysia; E-Mails:

出版信息

Int J Mol Sci. 2011;12(8):4872-84. doi: 10.3390/ijms12084872. Epub 2011 Aug 2.

Abstract

This paper presents the green synthesis of silver nanoparticles (Ag NPs) in aqueous medium. This method was performed by reducing AgNO(3) in different stirring times of reaction at a moderate temperature using green agents, chitosan (Cts) and polyethylene glycol (PEG). In this work, silver nitrate (AgNO(3)) was used as the silver precursor while Cts and PEG were used as the solid support and polymeric stabilizer. The properties of Ag/Cts/PEG nanocomposites (NCs) were studied under different stirring times of reaction. The developed Ag/Cts/PEG NCs were then characterized by the ultraviolet-visible (UV-Vis) spectroscopy, X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and Fourier transform infrared (FTIR) spectroscopy.

摘要

本文介绍了在水介质中绿色合成银纳米颗粒(Ag NPs)的方法。该方法是通过在适度温度下,使用绿色试剂壳聚糖(Cts)和聚乙二醇(PEG),在不同反应搅拌时间下还原硝酸银(AgNO₃)来实现的。在这项工作中,硝酸银(AgNO₃)用作银前驱体,而Cts和PEG分别用作固体载体和聚合物稳定剂。研究了不同反应搅拌时间下Ag/Cts/PEG纳米复合材料(NCs)的性能。然后通过紫外可见(UV-Vis)光谱、X射线衍射(XRD)、透射电子显微镜(TEM)、扫描电子显微镜(SEM)和傅里叶变换红外(FTIR)光谱对所制备的Ag/Cts/PEG NCs进行表征。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/46bb/3179138/cbd1f497fd39/ijms-12-04872f1.jpg

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