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壳聚糖、明胶及其壳聚糖/明胶纳米复合材料中通过化学还原剂合成银纳米粒子及其表征。

Synthesis of silver nanoparticles in chitosan, gelatin and chitosan/gelatin bionanocomposites by a chemical reducing agent and their characterization.

机构信息

Department of Chemistry, Faculty of Science, Universiti Putra Malaysia, UPM Serdang, Selangor 43400, Malaysia.

出版信息

Molecules. 2011 Aug 25;16(9):7237-48. doi: 10.3390/molecules16097237.

Abstract

In this research, silver nanoparticles (AgNPs) were synthesized in chitosan (Cts), Cts/gelatin and gelatin suspensions using a chemical reducing agent. Cts and gelatin were used as natural stabilizers and solid support, whereas AgNO(3) was used as the silver precursor. Sodium borohydride (NaBH(4)) was used as the reducing agent. The properties of AgNPs in Cts, Cts/gelatin and gelatin bionanocomposites (BNCs) were studied in terms of their surface plasmon resonance, crystalline structure, average diameter size, particle distributions, surface topography and functional groups. All the samples were characterized by UV-visible spectroscopy, powder X-ray diffraction, transmission electron microscopy, atomic force microscopy and Fourier transform infrared spectroscopy.

摘要

在这项研究中,使用化学还原剂在壳聚糖(Cts)、Cts/明胶和明胶悬浮液中合成了银纳米粒子(AgNPs)。壳聚糖和明胶被用作天然稳定剂和固体支撑物,而 AgNO3 则被用作银前体。使用硼氢化钠(NaBH4)作为还原剂。通过紫外-可见光谱、粉末 X 射线衍射、透射电子显微镜、原子力显微镜和傅里叶变换红外光谱研究了 Cts、Cts/明胶和明胶生物纳米复合材料(BNCs)中 AgNPs 的表面等离子体共振、晶体结构、平均粒径、颗粒分布、表面形貌和官能团。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a547/6264134/e0cc812eb8ec/molecules-16-07237-g001.jpg

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