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机械合金化和高频感应加热烧结制备 Ti-Nb-Sn-羟基磷灰石复合材料。

Ti-Nb-Sn-hydroxyapatite composites synthesized by mechanical alloying and high frequency induction heated sintering.

机构信息

National Key Laboratory of Science and Technology on Precision Heat Processing of Metals, Harbin Institute of Technology, Harbin 150001, China.

出版信息

J Mech Behav Biomed Mater. 2011 Nov;4(8):2074-80. doi: 10.1016/j.jmbbm.2011.07.006. Epub 2011 Jul 22.

Abstract

A β-type Ti-based composite, Ti-35Nb-2.5Sn-15-hydroxyapatite (HA), has been synthesized by mechanical alloying and powder metallurgy. The effects of milling time on microstructure, mechanical properties and biocompatibility of the sintered composites were investigated by scanning electronic microscopy (SEM), X-ray diffraction (XRD), microhardness tests, compression tests and cells culture. The results revealed when milling time increased, the homogeneity and relative density of the sintered composite increased, but the finished sintering temperature decreased. The compression Young's modulus of sintered composite from 12 h milled powders was about 22 GPa and its compression strength was 877 MPa. The cell culture results indicated cell viability for these sintered composites was very good. These results revealed the Ti-35Nb-2.5Sn-15HA composite could be useful for medical implants.

摘要

通过机械合金化和粉末冶金法合成了一种β型 Ti 基复合材料 Ti-35Nb-2.5Sn-15HA。采用扫描电子显微镜(SEM)、X 射线衍射(XRD)、显微硬度试验、压缩试验和细胞培养等方法研究了球磨时间对烧结复合材料的微观结构、力学性能和生物相容性的影响。结果表明,随着球磨时间的增加,烧结复合材料的均匀性和相对密度增加,而最终烧结温度降低。12 h 球磨粉末烧结复合材料的压缩杨氏模量约为 22 GPa,压缩强度为 877 MPa。细胞培养结果表明,这些烧结复合材料的细胞活力非常好。这些结果表明 Ti-35Nb-2.5Sn-15HA 复合材料可用于医疗植入物。

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