Centro de Investigaciones Químicas, Universidad Autónoma del Estado de Morelos, Av. Universidad 1001, Cuernavaca, Mor., CP 62209, Mexico.
Molecules. 2011 Dec 27;17(1):151-62. doi: 10.3390/molecules17010151.
We describe a protocol developed for the preparation of β-enaminoketones derived from 1,3-cyclohexanediones, and their subsequent reduction by sodium in THF-isopropyl alcohol to afford cis- and trans-3-aminocyclohexanols.
我们描述了一种从 1,3-环己二酮制备β-烯胺酮的方法,以及它们随后在四氢呋喃-异丙醇中被钠还原为顺式和反式-3-氨基环己醇。