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使用不同pH值的自酸蚀粘结剂评估树脂复合材料与玻璃离子水门汀的剪切粘结强度:体外研究。

Shear bond strength evaluation of resin composite bonded to glass-ionomer cement using self-etching bonding agents with different pH: In vitro study.

作者信息

Kandaswamy Deivanayagam, Rajan Karunamoorthy Jeyavel, Venkateshbabu Nagendrababu, Porkodi Ilango

机构信息

Department of Conservative Dentistry and Endodontics, Faculty of Dental Sciences, Sri Ramachandra University, Porur, Chennai, India.

出版信息

J Conserv Dent. 2012 Jan;15(1):27-31. doi: 10.4103/0972-0707.92602.

Abstract

AIM

To evaluate the bonding ability of composite to unset glass-ionomer cement (GIC) using different self-etching bonding systems.

MATERIALS AND METHODS

One hundred samples of composite bonded to unset GIC were prepared and were divided into four groups. In Group A, composite was bonded to unset GIC employing a strong (pH 1) self-etch primer was used. In Group B, intermediary strong (pH 1.4) self-etch primer was employed. In Group C and D, mild (pH 2) and (pH 2.2) self-etch primer was employed. Shear bond strength analysis was performed at a cross-head speed of 0.5 mm/min.

RESULTS

Statistical analysis performed with one way analysis of variance and Tukey's test showed that the bond strength of composite to unset GIC was significantly higher for the mild self-etch primer group. In addition, energy dispersive x-ray (EDX) analysis was used to determine the composition of various structural phases identified by FE-SEM along the GIC-bonding agent interfaces.

CONCLUSION

Hence this present study concludes that clinically the use of mild self-etching bonding agent over unset GIC has improved bond strength compared to the use of strong and intermediate self-etching bonding agent.

摘要

目的

使用不同的自酸蚀粘结系统评估复合树脂与未凝固玻璃离子水门汀(GIC)的粘结能力。

材料与方法

制备100个复合树脂粘结到未凝固GIC的样本,并分为四组。A组中,复合树脂采用强酸性(pH 1)自酸蚀底漆粘结到未凝固GIC上。B组采用中等强度(pH 1.4)自酸蚀底漆。C组和D组分别采用弱酸性(pH 2)和(pH 2.2)自酸蚀底漆。以0.5 mm/min的十字头速度进行剪切粘结强度分析。

结果

采用单因素方差分析和Tukey检验进行的统计分析表明,弱酸性自酸蚀底漆组中复合树脂与未凝固GIC的粘结强度显著更高。此外,能量色散X射线(EDX)分析用于确定通过场发射扫描电子显微镜(FE-SEM)在GIC-粘结剂界面处识别的各种结构相的组成。

结论

因此,本研究得出结论,临床上与使用强酸性和中等强度自酸蚀粘结剂相比,在未凝固GIC上使用弱酸性自酸蚀粘结剂可提高粘结强度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a0d0/3284008/7ba65e80ac2d/JCD-15-27-g003.jpg

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