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使用不同pH值的自酸蚀粘合剂和全酸蚀粘合剂评估纳米填充复合材料与玻璃离子水门汀之间的剪切粘结强度。

Assessment of the Shear Bond Strength between Nanofilled Composite Bonded to Glass-ionomer Cement Using Self-etch Adhesive with Different pHs and Total-Etch Adhesive.

作者信息

Sharafeddin Farahnaz, Choobineh Mohammad Mehdi

机构信息

Dept. of Operative Dentistry, Biomaterials Research Center, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.

Undergraduate Student, School of Dentistry, International Branch of Shiraz University of Medical Sciences, Shiraz, Iran.

出版信息

J Dent (Shiraz). 2016 Mar;17(1):1-6.

PMID:26966701
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC4771046/
Abstract

STATEMENT OF THE PROBLEM

In the sandwich technique, the undesirable bond between the composite resin and glass-ionomer cement (GIc) is one of the most important factors which lead to the failure of restoration. Total-etch and self-etch adhesives may improve the bond strength based on their pH.

PURPOSE

The purpose of this study was to evaluate the shear bond strength between the nanofilled composite resin and GIc using different adhesives.

MATERIALS AND METHOD

In this experimental study, 40 specimens (6×6mm) in 4 groups (n=10) were prepared in acrylic mold. Each specimen contained conventional GI ChemFil Superior with a height of 3mm, bonded to Z350 composite resin with a height measured 3mm. In order to bond the composite to the GI, the following adhesives were used, respectively: A: mild Clearfil SE Bond self-etch (pH=2), B: intermediate OptiBond self-etch (pH=1.4), C: strong Adper Prompt L-Pop (pH=1), and D: Adper Single Bond 2 total-etch (pH=7.2). The shear bond strength was measured by using universal testing machine with a crosshead speed of 1mm/min. One-way ANOVA and Tukey's test were used to analyze the data (p< 0.05).

RESULTS

The shear bond strength in group A was significantly higher than group B (p= 0.002), C (p< 0.001), and D (p< 0.001). Moreover, the shear bond strength of groups A and B (self-etch) was significantly different from group D (total-etch) (p< 0.001); and C (self-etch) with D (p= 0.024).

CONCLUSION

The results of this study showed that applying the mild self-etch adhesive between the composite and the GIc results in stronger shear bond strength compared to intermediate and strong self-etch adhesives. Moreover, the self-etch adhesive increased the shear bond strength between composite resin and GIc more significantly than total-etch adhesive.

摘要

问题陈述

在三明治技术中,复合树脂与玻璃离子水门汀(GIc)之间不良的粘结是导致修复失败的最重要因素之一。全酸蚀和自酸蚀粘结剂可根据其pH值提高粘结强度。

目的

本研究的目的是使用不同的粘结剂评估纳米填充复合树脂与GIc之间的剪切粘结强度。

材料与方法

在本实验研究中,在丙烯酸模具中制备了4组(n = 10)共40个试件(6×6mm)。每个试件包含高度为3mm的传统GI ChemFil Superior,与高度为3mm的Z350复合树脂粘结。为了将复合材料粘结到GI上,分别使用了以下粘结剂:A:温和型Clearfil SE Bond自酸蚀粘结剂(pH = 2),B:中等强度型OptiBond自酸蚀粘结剂(pH = 1.4),C:高强度型Adper Prompt L-Pop(pH = 1),以及D:Adper Single Bond 2全酸蚀粘结剂(pH = 7.2)。使用万能试验机以1mm/min的十字头速度测量剪切粘结强度。采用单因素方差分析和Tukey检验对数据进行分析(p < 0.05)。

结果

A组的剪切粘结强度显著高于B组(p = 0.002)、C组(p < 0.001)和D组(p < 0.001)。此外,A组和B组(自酸蚀)的剪切粘结强度与D组(全酸蚀)有显著差异(p < 0.001);C组(自酸蚀)与D组相比也有差异(p = 0.024)。

结论

本研究结果表明,与中等强度和高强度自酸蚀粘结剂相比,在复合材料和GIc之间应用温和型自酸蚀粘结剂可获得更强的剪切粘结强度。此外,自酸蚀粘结剂比全酸蚀粘结剂更显著地提高了复合树脂与GIc之间的剪切粘结强度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4328/4771046/0a4bf1a05815/jds-17-1-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4328/4771046/d835a7e1c3ec/jds-17-1-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4328/4771046/2cdcb33ced93/jds-17-1-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4328/4771046/0a4bf1a05815/jds-17-1-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4328/4771046/d835a7e1c3ec/jds-17-1-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4328/4771046/2cdcb33ced93/jds-17-1-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4328/4771046/0a4bf1a05815/jds-17-1-g003.jpg

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