Kim Y-R, Chen P, Aziz M J, Branton D, Vlassak J J
J Appl Phys. 2006 Nov 15;100(10):104322-104330. doi: 10.1063/1.2363900.
Prominent deflections are shown to occur in freestanding silicon nitride thin membranes when exposed to a 50 keV gallium focused ion beam for ion doses between 10(14) and 10(17) ions/cm(2). Atomic force microscope topographs were used to quantify elevations on the irradiated side and corresponding depressions of comparable magnitude on the back side, thus indicating that what at first appeared to be protrusions are actually the result of membrane deflections. The shape in high-stress silicon nitride is remarkably flattopped and differs from that in low-stress silicon nitride. Ion beam induced biaxial compressive stress generation, which is a known deformation mechanism for other amorphous materials at higher ion energies, is hypothesized to be the origin of the deflection. A continuum mechanical model based on this assumption convincingly reproduces the profiles for both low-stress and high-stress membranes and provides a family of unusual shapes that can be created by deflection of freestanding thin films under beam irradiation.
当暴露于能量为50 keV的镓聚焦离子束下,离子剂量在10(14)至10(17)离子/cm(2)之间时,独立的氮化硅薄膜中会出现明显的偏转。使用原子力显微镜地形图来量化辐照侧的凸起以及背面相应的大小相当的凹陷,从而表明最初看似突起的实际上是薄膜偏转的结果。高应力氮化硅中的形状明显呈平顶,与低应力氮化硅中的形状不同。离子束诱导的双轴压缩应力产生被假设为偏转的起源,这是其他非晶材料在较高离子能量下已知的变形机制。基于此假设的连续介质力学模型令人信服地再现了低应力和高应力薄膜的轮廓,并提供了一系列可通过束辐照下独立薄膜的偏转产生的异常形状。