Physikalisch-Technische Bundesanstalt, Braunschweig, Germany.
Small. 2012 Sep 10;8(17):2675-9. doi: 10.1002/smll.201200420. Epub 2012 Jun 22.
The quantitative measurement of the magnetization of individual magnetic nanoparticles (MNPs) using magnetic force microscopy (MFM) is described. Quantitative measurement is realized by calibration of the MFM signal using an MNP reference sample with traceably determined magnetization. A resolution of the magnetic moment of the order of 10(-18) A m(2) under ambient conditions is demonstrated, which is presently limited by the tip's magnetic moment and the noise level of the instrument. The calibration scheme can be applied to practically any magnetic force microscope and tip, thus allowing a wide range of future applications, for example in nanomagnetism and biotechnology.
本文描述了使用磁力显微镜(MFM)对单个磁性纳米粒子(MNPs)的磁化进行定量测量的方法。通过使用具有可追溯确定磁化的 MNPs 参考样品对 MFM 信号进行校准,实现了定量测量。在环境条件下,演示了分辨率约为 10(-18) A m(2)的磁矩,目前该分辨率受到探针磁矩和仪器噪声水平的限制。该校准方案可应用于几乎任何磁力显微镜和探针,因此可以实现广泛的未来应用,例如在纳米磁学和生物技术中。