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表面后处理对自粘型粘结剂粘结强度的影响。

Effects of post surface treatments on the bond strength of self-adhesive cements.

作者信息

Mazzitelli Claudia, Papacchini Federica, Monticelli Francesca, Toledano Manuel, Ferrari Marco

机构信息

Department of Fixed Prosthodontics and Dental Materials, School of Dental Medicine, Policlinico "Le Scotte", University of Siena, viale Bracci 1, Siena, 53100, Italy.

出版信息

Am J Dent. 2012 Jun;25(3):159-64.

Abstract

PURPOSE

To evaluate whether fiber post surface conditioning techniques would influence the ultimate retentive strength of self-adhesive resin cements into the root canal.

METHODS

50 single-rooted premolars with one root canal were endodontically treated and prepared to receive a fiber post. Five groups were formed (n=10) according to the post surface pre-treatment performed: (1) Silane application (Monobond S) for 60 seconds; (2) 10% hydrogen peroxide application for 20 minutes; (3) Rocatec Pre; (4) Silicate/silane coating (DT Light SL Post); (5) No treatment (DT Light Post). Two self-adhesive resin cements (RelyX Unicem and MaxCem) were used as luting agents. The bonded specimens were stored up to 1 month (37 degrees C and 100% humidity). The force required to dislodge the post (MPa) via an apical-coronal direction was measured with the push-out bond strength test (cross-head speed: 0.5 mm/minute until failure). Failure patterns were evaluated under SEM. Data was statistically analyzed with one-way ANOVA and Tukey tests (P< 0.05).

RESULTS

No increase in the push-out bond strength values were observed for RelyX Unicem, independently from the post surface treatment performed. MaxCem attained higher bond strengths when luted to silanated posts.

摘要

目的

评估纤维桩表面处理技术是否会影响自粘接树脂水门汀在根管内的最终固位强度。

方法

选取50颗单根管前磨牙进行根管治疗并预备以容纳纤维桩。根据桩表面预处理方式分为五组(n = 10):(1)硅烷处理(Monobond S)60秒;(2)10%过氧化氢处理20分钟;(3)Rocatec Pre;(4)硅酸盐/硅烷涂层(DT Light SL桩);(5)不处理(DT Light桩)。使用两种自粘接树脂水门汀(RelyX Unicem和MaxCem)作为粘接剂。粘接后的标本在37℃、100%湿度下储存长达1个月。通过推出粘结强度试验(十字头速度:0.5毫米/分钟直至破坏)测量沿根尖-冠方方向推出桩所需的力(MPa)。在扫描电子显微镜下评估失败模式。数据采用单因素方差分析和Tukey检验进行统计学分析(P < 0.05)。

结果

无论对桩进行何种表面处理,RelyX Unicem的推出粘结强度值均未增加。当MaxCem与硅烷化处理的桩粘结时,获得了更高的粘结强度。

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