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一步法绿色合成与表征麻藤叶介导的生物相容性银和金纳米粒子

One-step green synthesis and characterization of leaf extract-mediated biocompatible silver and gold nanoparticles from Memecylon umbellatum.

机构信息

Center for Environmental Nuclear Research, Directorate of Research, SRM University, Chennai, Tamil Nadu, India.

出版信息

Int J Nanomedicine. 2013;8:1307-15. doi: 10.2147/IJN.S36670. Epub 2013 Mar 26.

Abstract

In this experiment, green-synthesized silver and gold nanoparticles were produced rapidly by treating silver and gold ions with an extract of Memecylon umbellatum leaf. The reaction process was simple and easy to handle, and was monitored using ultraviolet-visible spectroscopy. The effect of the phytochemicals present in M. umbellatum, including saponins, phenolic compounds, phytosterols, and quinones, on formation of stable silver and gold nanoparticles was investigated by Fourier-transform infrared spectroscopy. The morphology and crystalline phase of the nanoparticles were determined by transmission electron microscopy and energy-dispersive x-ray spectroscopy. The results indicate that the saponins, phytosterols, and phenolic compounds present in the plant extract play a major role in formation of silver and gold nanoparticles in their respective ions in solution. The characteristics of the nanoparticles formed suggest application of silver and gold nanoparticles as chemical sensors in the future. Given the simple and eco-friendly approach for synthesis, these nanoparticles could easily be commercialized for large-scale production.

摘要

在这项实验中,通过用 Memecylon umbellatum 叶的提取物处理银离子和金离子,快速制备了绿色合成的银和金纳米粒子。反应过程简单且易于操作,并通过紫外-可见光谱进行监测。通过傅里叶变换红外光谱研究了 M.umbellatum 中存在的植物化学物质,包括皂苷、酚类化合物、植物甾醇和醌类化合物,对形成稳定的银和金纳米粒子的影响。通过透射电子显微镜和能量色散 X 射线能谱确定了纳米粒子的形态和晶体相。结果表明,植物提取物中的皂苷、植物甾醇和酚类化合物在溶液中各自的离子中形成银和金纳米粒子方面发挥了主要作用。形成的纳米粒子的特性表明,将来可以将银和金纳米粒子用作化学传感器。鉴于合成方法简单且环保,这些纳米粒子可以很容易地进行商业化大规模生产。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1fb6/3615924/8612354caedc/ijn-8-1307Fig1.jpg

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