Department of Chemistry and Biotechnology, Tottori University, Tottori 680-8502, Japan.
Carbohydr Polym. 2013 Sep 12;97(2):363-7. doi: 10.1016/j.carbpol.2013.05.010. Epub 2013 May 13.
Chitosan nanofibers were easily prepared from dry chitosan powder using the Star Burst system, which employs a high-pressure water jet system. Although the chitosan nanofibers became thinner as the number of Star Burst passes increased, the fiber thickness did not change significantly above 10 passes. Crystallinity and the chitosan nanofiber length decreased after extensive treatment due to the strong collision forces breaking the fibers. The mechanical properties and thermal expansion of the chitosan nanofiber sheets were improved by increasing the number of passes up to 10, but further treatment resulted in a deterioration of these properties.
壳聚糖纳米纤维很容易从干壳聚糖粉末通过采用高压水射流系统的星爆系统制备得到。虽然随着星爆通过次数的增加壳聚糖纳米纤维变得更细,但在 10 次以上通过时纤维厚度没有明显变化。由于强烈的碰撞力会破坏纤维,因此在经过广泛处理后,结晶度和壳聚糖纳米纤维长度都会降低。通过增加通过次数至 10 次,可以提高壳聚糖纳米纤维片的机械性能和热膨胀性能,但进一步处理会导致这些性能恶化。