采用傅里叶变换红外光谱法测定药物制剂中的橙皮苷。
Determination of diosmin in pharmaceutical formulations using Fourier transform infrared spectrophotometry.
机构信息
Cromatec_plus srl, Analytical Research Department, 18 Sos. Cotroceni, Bucharest 6, 060114, Romania.
出版信息
Saudi Pharm J. 2009 Oct;17(4):303-6. doi: 10.1016/j.jsps.2009.10.008. Epub 2009 Nov 10.
Abstract
A Fourier transform infrared (FT-IR) spectrometric method was developed for the rapid, direct measurement of diosmin in different pharmaceutical drugs. Conventional KBr-spectra were compared for best determination of active substance in commercial preparations. The Beer-Lambert law and two chemometric approaches, partial least squares (PLS) and principal component regression (PCR+) methods, were tried in data processing.
摘要
建立了一种傅里叶变换红外（FT-IR）光谱法，用于快速、直接测定不同药物制剂中的地奥司明。比较了常规的 KBr 光谱，以确定商业制剂中活性物质的最佳测定方法。在数据处理中尝试了 Beer-Lambert 定律和两种化学计量学方法，即偏最小二乘法（PLS）和主成分回归（PCR+）方法。
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