Oladele Isiaka Oluwole, Adewole Temitope Akinyemi
Department of Metallurgical and Materials Engineering, Federal University of Technology, Akure, Nigeria.
Biotechnol Res Int. 2013;2013:725396. doi: 10.1155/2013/725396. Epub 2013 Nov 14.
This work was carried out to investigate the influence of cow bone particle size distribution on the mechanical properties of polyester matrix composites in order to consider the suitability of the materials as biomaterials. Cow bone was procured from an abattoir, washed with water, and sun-dried for 4 weeks after which it was crushed with a sledge hammer and was further pulverized with laboratory ball mill. Sieve size analysis was carried out on the pulverized bone where it was sieved into three different sizes of 75, 106, and 300 μm sieve sizes. Composite materials were developed by casting them into tensile and flexural tests moulds using predetermined proportions of 2, 4, 6, and 8%. The samples after curing were striped from the moulds and were allowed to be further cured at room temperature for 3 weeks before tensile and flexural tests were performed on them. Both tensile and flexural strength were highly enhanced by 8 wt% from 75 μm while toughness was highly enhanced by 6 and 8 wt% from 300 μm. This shows that fine particles lead to improved strength while coarse particles lead to improved toughness. The results show that these materials are structurally compatible and are being developed from animal fibre based particle; it is expected to also aid the compatibility with the surface conditions as biomaterials.
开展这项工作是为了研究牛骨粒度分布对聚酯基复合材料力学性能的影响,以便考虑这些材料作为生物材料的适用性。牛骨从屠宰场采购,用水冲洗,然后日晒4周,之后用大锤粉碎,并在实验室球磨机中进一步研磨。对研磨后的骨头进行筛析,将其筛分成75、106和300μm三种不同尺寸。使用2%、4%、6%和8%的预定比例将复合材料浇铸到拉伸和弯曲试验模具中制成。固化后的样品从模具中取出,在室温下进一步固化3周,然后对其进行拉伸和弯曲试验。75μm的颗粒使拉伸强度和弯曲强度均提高了8 wt%,而300μm的颗粒使韧性分别提高了6 wt%和8 wt%。这表明细颗粒可提高强度,而粗颗粒可提高韧性。结果表明,这些材料在结构上具有相容性,且由动物纤维基颗粒制成;预计这也有助于作为生物材料与表面条件的相容性。