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光照对光固化复合材料断裂韧性和弯曲强度的影响。

Effect of light exposure on fracture toughness and flexural strength of light-cured composites.

作者信息

Miyazaki M, Oshida Y, Moore B K, Onose H

机构信息

Department of Operative Dentistry, Nihon University School of Dentistry, Tokyo, Japan.

出版信息

Dent Mater. 1996 Nov;12(6):328-32. doi: 10.1016/s0109-5641(96)80042-x.

Abstract

OBJECTIVES

This study was conducted to investigate the curing characteristics of light-cured composites and their related mechanical properties.

METHODS

Single-edge notch specimens [25 mm x 2.5 mm x 5 mm with a 5 mm notch (a/W = 0.5)] were prepared for fracture toughness measurements. For flexural strength testing, a stainless steel mold (25 mm x 2 mm x 2 mm) was used. Light-cured composites were condensed into the mold, and the middle third of the specimen was first activated for 30 s with 400 mW/cm2, for 60 s with 200 mW/cm2, or for 120 s with 100 mW/cm2. Then the remaining thirds were activated at the same intensity and curing time as the middle third. After 24 h storage in 37 degrees C water, three-point bending tests were performed with a span length of 20 mm at a crosshead speed of 0.5 mm/min. A one-way ANOVA, followed by a Newman-Keuls test (p < 0.05), were used to compare the data obtained from each group to test the effect of the curing conditions.

RESULTS

Fracture toughness, flexural strength, and flexural modulus varied with resin composites. Among the three curing conditions for each material, there were no significant differences in fracture toughness, flexural strength, or flexural modulus.

SIGNIFICANCE

The fracture toughness and the flexural strength were the same when irradiations with the same amount of energy (light intensity multiplied by curing time) were used. It was found that, at lower light intensity, longer curing was required to provide comparable mechanical properties. An accumulated irradiation energy obtained through a product of the light intensity and curing time may serve as a guideline to produce samples exhibiting equivalent fracture toughness as well as flexural strengths.

摘要

目的

本研究旨在调查光固化复合材料的固化特性及其相关力学性能。

方法

制备单边缺口试样[25毫米×2.5毫米×5毫米,带有5毫米缺口(a/W = 0.5)]用于断裂韧性测量。对于弯曲强度测试,使用不锈钢模具(25毫米×2毫米×2毫米)。将光固化复合材料填入模具中,试样的中间三分之一首先用400毫瓦/平方厘米的强度照射30秒,或用200毫瓦/平方厘米的强度照射60秒,或用100毫瓦/平方厘米的强度照射120秒。然后其余三分之一以与中间三分之一相同的强度和固化时间进行照射。在37℃水中储存24小时后,以0.5毫米/分钟的十字头速度在20毫米的跨度下进行三点弯曲试验。使用单向方差分析,随后进行纽曼-基尔斯检验(p < 0.05),以比较从每组获得的数据,测试固化条件的影响。

结果

断裂韧性、弯曲强度和弯曲模量随树脂复合材料而变化。对于每种材料的三种固化条件,断裂韧性、弯曲强度或弯曲模量没有显著差异。

意义

当使用相同能量(光强度乘以固化时间)照射时,断裂韧性和弯曲强度相同。结果发现,在较低光强度下,需要更长的固化时间以提供相当的力学性能。通过光强度和固化时间的乘积获得的累积照射能量可作为生产具有等效断裂韧性和弯曲强度的样品的指导。

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