UER Chimie appliquée, Ecole Militaire Polytechnique, BP 17, Alger, Algeria.
LERMAB, Faculté des Sciences et Technologies, Université de Lorraine, Vandœuvre-lès-Nancy, France.
Carbohydr Polym. 2014 Apr 15;104:223-30. doi: 10.1016/j.carbpol.2014.01.058. Epub 2014 Jan 27.
In this study, microcrystalline cellulose (Alfa-MCC) was extracted from Alfa fibres using acid hydrolysis method. The molecular weight of the cellulose samples was determined by gel permeation chromatography. The crystallinities were studied by means of X-ray diffraction and solid state cross polarization magic angle spinning (13)C nuclear magnetic resonance spectroscopy, revealing that Alfa-MCC was more crystalline than the native cellulose isolated from Alfa fibres. The morphology of the celluloses was investigated using scanning electron microscopy, showing a compact structure and a rough surface. Furthermore, a good thermal stability was shown for Alfa-MCC. Based on these analyses, Alfa-MCC showed tremendous potential use as composites reinforcing agent, foods stabilizer and pharmaceutical additive.
在这项研究中,使用酸水解法从 Alfa 纤维中提取微晶纤维素(Alfa-MCC)。通过凝胶渗透色谱法测定纤维素样品的分子量。通过 X 射线衍射和固态交叉极化魔角旋转(13)C 核磁共振波谱研究了结晶度,结果表明 Alfa-MCC 比从 Alfa 纤维中分离出的天然纤维素具有更高的结晶度。使用扫描电子显微镜研究了纤维素的形态,显示出致密的结构和粗糙的表面。此外,Alfa-MCC 表现出良好的热稳定性。基于这些分析,Alfa-MCC 显示出作为复合材料增强剂、食品稳定剂和药物添加剂的巨大应用潜力。