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氧化镁纳米线的新型大规模合成:结构与抗菌性能

A new large - Scale synthesis of magnesium oxide nanowires: Structural and antibacterial properties.

作者信息

Al-Hazmi Faten, Alnowaiser Fowzia, Al-Ghamdi A A, Al-Ghamdi Attieh A, Aly M M, Al-Tuwirqi Reem M, El-Tantawy Farid

机构信息

Department of Physics, Faculty of Sciences, King Abdulaziz University, Jeddah, Saudi Arabia.

Chemistry Department, Faculty of Sciences, King Abdulaziz University, Jeddah, Saudi Arabia.

出版信息

Superlattices Microstruct. 2012 Aug;52(2):200-209. doi: 10.1016/j.spmi.2012.04.013.

Abstract

Large-scale one-dimensional magnesium oxide (MgO) nanowires with diameters of 6 nm and lengths of 10 μm have been successfully synthesized by a new facile and simple reaction. This production was performed via a microwave hydrothermal approach at low temperature growth of 180 °C for 30 min. The structure of as synthesized MgO nanowires were investigated by means of X-ray diffraction (X-ray), Fourier Transformation Infrared Spectroscopy (FTIR), Field Emission Scanning Electron Microscopy (FE-SEM), Transmission Electron Microscopy (TEM), Selected Area Electron Diffraction (SAED) and Energy Dispersive X-ray (EDS). The antibacterial behavior of MgO nanowires concentration in solid media against Gram negative and Gram positive for different bacteria has been tested in details. The results show that the MgO nanowires have bacteriostatic activity against and Bacillus sp. The antibacterial activity increases with increasing MgO nanowires concentration. Furthermore, the presence of one-dimensional MgO nanowires has high antibacterial efficacy and damages the membrane wall of bacteria. Finally, this study offered the prospect of developing ultrafine nanoscale devices utilizing MgO nanowires and implementing their useful potential in biological control.

摘要

通过一种新的简便反应,成功合成了直径为6纳米、长度为10微米的大规模一维氧化镁(MgO)纳米线。该制备过程是通过微波水热法在180°C的低温下生长30分钟来进行的。采用X射线衍射(X射线)、傅里叶变换红外光谱(FTIR)、场发射扫描电子显微镜(FE-SEM)、透射电子显微镜(TEM)、选区电子衍射(SAED)和能量色散X射线(EDS)对合成的氧化镁纳米线结构进行了研究。详细测试了固体培养基中不同浓度的氧化镁纳米线对革兰氏阴性菌和革兰氏阳性菌的抗菌行为。结果表明,氧化镁纳米线对[具体细菌名称未给出]和芽孢杆菌具有抑菌活性。抗菌活性随氧化镁纳米线浓度的增加而增强。此外,一维氧化镁纳米线的存在具有很高的抗菌效果,并会破坏细菌的细胞膜壁。最后,本研究为利用氧化镁纳米线开发超细纳米级器件并实现其在生物控制中的有用潜力提供了前景。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/26c2/3990453/fdd39ebfac7e/gr1.jpg

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