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蒸气冷凝辅助光学显微镜观察超长碳纳米管和其他纳米结构。

Vapor-condensation-assisted optical microscopy for ultralong carbon nanotubes and other nanostructures.

机构信息

State Key Laboratory of Low-Dimensional Quantum Physics, Department of Physics and Tsinghua-Foxconn Nanotechnology Research Center, Tsinghua University , Beijing 100084, China.

出版信息

Nano Lett. 2014 Jun 11;14(6):3527-33. doi: 10.1021/nl5016969. Epub 2014 May 28.

DOI:10.1021/nl5016969
PMID:24854098
Abstract

Here we present a simple yet powerful approach for the imaging of nanostructures under an optical microscope with the help of vapor condensation on their surfaces. Supersaturated water vapor will first form a nanometer-sized water droplet on the condensation nuclei on the surface of nanostructures, and then the water droplet will grow bigger and scatter more light to make the outline of the nanostructure be visible under dark-field optical microscope. This vapor-condensation-assisted (VCA) optical microscopy is applicable to a variety of nanostructures from ultralong carbon nanotubes to functional groups, generating images with contrast coming from the difference in density of the condensation sites, and does not induce any impurities to the specimens. Moreover, this low-cost and efficient technique can be conveniently integrated with other facilities, such as Raman spectroscope and so forth, which will pave the way for widespread applications.

摘要

在这里,我们提出了一种简单而强大的方法,通过在纳米结构表面的蒸汽冷凝作用,在光学显微镜下对纳米结构进行成像。过饱和水蒸气将首先在纳米结构表面的冷凝核上形成纳米级的小水滴,然后小水滴会变大并散射更多的光,使得纳米结构的轮廓在暗场光学显微镜下可见。这种蒸气冷凝辅助(VCA)光学显微镜适用于从超长碳纳米管到官能团等各种纳米结构,其图像对比度来自于冷凝点密度的差异,且不会给样品带来任何杂质。此外,这种低成本、高效率的技术可以方便地与其他设备(如拉曼光谱仪等)集成,为广泛应用铺平道路。

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Nano Lett. 2014 Jun 11;14(6):3527-33. doi: 10.1021/nl5016969. Epub 2014 May 28.
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引用本文的文献

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Optical visualization and imaging of nanomaterials.纳米材料的光学可视化与成像
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2
Nanoarray-Embedded Hierarchical Surfaces for Highly Durable Dropwise Condensation.用于高度持久滴状冷凝的纳米阵列嵌入式分级表面
Research (Wash D C). 2022 Aug 9;2022:9789657. doi: 10.34133/2022/9789657. eCollection 2022.
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Rate-selected growth of ultrapure semiconducting carbon nanotube arrays.超高纯半导体碳纳米管阵列的择优生长。
Nat Commun. 2019 Oct 2;10(1):4467. doi: 10.1038/s41467-019-12519-5.
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Probing photoresponse of aligned single-walled carbon nanotube doped ultrathin MoS.探测取向排列的单壁碳纳米管掺杂超薄二硫化钼的光响应
Nanotechnology. 2018 Aug 24;29(34):345205. doi: 10.1088/1361-6528/aaca69. Epub 2018 Jun 5.
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Acoustic-assisted assembly of an individual monochromatic ultralong carbon nanotube for high on-current transistors.声学辅助组装单根单色超长碳纳米管用于高导通电流晶体管。
Sci Adv. 2016 Nov 30;2(11):e1601572. doi: 10.1126/sciadv.1601572. eCollection 2016 Nov.