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各种氟化物制剂对未涂层、镀铑和硝化镍钛正畸丝的工作性能及表面特性的影响

Influence of various fluoride agents on working properties and surface characteristics of uncoated, rhodium coated and nitrified nickel-titanium orthodontic wires.

作者信息

Katić Višnja, Mandić Vilko, Ježek Damir, Baršić Gorana, Špalj Stjepan

机构信息

Department of Orthodontics, Faculty of Medicine, University of Rijeka , Rijeka , Croatia.

出版信息

Acta Odontol Scand. 2015 May;73(4):241-9. doi: 10.3109/00016357.2014.980847. Epub 2015 Feb 2.

Abstract

OBJECTIVE

To analyze the effect of various fluoride formulations in commercially available agents on working properties of various nickel-titanium orthodontic wires.

MATERIALS AND METHODS

Uncoated (NiTi), rhodium coated (RhNiTi) and nitrified (NNiTi) wires were immersed to dH2O, MiPaste, Elmex and Mirafluor for 1 h. Unloading slope characteristics (average force, bending action of the force and average plateau length) and the percentage of useable constant force during unloading were observed. Surface roughness (Ra) was measured. SEM and EDS were used for observation of the surface.

RESULTS

NiTi had decreased loading and unloading elastic modulus (E) and yield strength (YS) after immersion to MIPaste and Mirafluor. The unloading YS decreased in the RhNiTi by the MIPaste. The loading and unloading YS of the NNiTi increased in Elmex and increased average plateau force. RhNiTi showed higher average plateau length and the percentage of useful constant force during unloading in Mirafluor and the average plateau force lowered after immersion to MIPaste. The unloading slope characteristics for NiTi were affected by all three prophylactic agents, mostly by Mirafluor, and produced significantly lower forces during both loading and unloading, similarly to the NNiTi wires. The RhNiTi had the lowest forces during both loading and unloading in MIPaste. All results were at significance; p<0.05. Difference in Ra was observed for RhNiTi after immersion to the MI Paste (p<0.001; η2=0.761).

CONCLUSION

The NiTi and NNiTi wires lose less working force when combined with Elmex. The RhNiTi improve their working properties with Mirafluor and deteriorate when combined with MiPaste.

摘要

目的

分析市售含氟制剂中不同氟化物配方对各种镍钛正畸丝工作性能的影响。

材料与方法

将未涂层(NiTi)、镀铑(RhNiTi)和渗氮(NNiTi)的正畸丝分别浸入去离子水、MiPaste、Elmex和Mirafluor中1小时。观察卸载斜率特性(平均力、力的弯曲作用和平均平台长度)以及卸载过程中可用恒力的百分比。测量表面粗糙度(Ra)。使用扫描电子显微镜(SEM)和能谱仪(EDS)观察表面情况。

结果

NiTi丝浸入MiPaste和Mirafluor后,加载和卸载弹性模量(E)以及屈服强度(YS)降低。RhNiTi丝浸入MiPaste后卸载YS降低。NNiTi丝浸入Elmex后加载和卸载YS增加,平均平台力增加。RhNiTi丝在Mirafluor中卸载时平均平台长度更长,可用恒力百分比更高,浸入MiPaste后平均平台力降低。NiTi丝的卸载斜率特性受到所有三种预防剂的影响,主要是Mirafluor,加载和卸载过程中产生的力显著降低,与NNiTi丝类似。RhNiTi丝在MiPaste中加载和卸载时的力最低。所有结果均具有显著性;p<0.05。RhNiTi丝浸入MI Paste后观察到Ra有差异(p<0.001;η2=0.761)。

结论

NiTi和NNiTi丝与Elmex联合使用时工作力损失较小。RhNiTi丝与Mirafluor联合使用时工作性能改善,与MiPaste联合使用时性能变差。

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