a SCIENT by CROMATEC_PLUS SRL, Research Center for Instrumental Analysis , Bucharest , Romania.
Crit Rev Anal Chem. 2015;45(4):289-99. doi: 10.1080/10408347.2014.949616.
X-ray diffraction (XRD) is a powerful nondestructive technique for characterizing crystalline materials. It provides information on structures, phases, preferred crystal orientations (texture), and other structural parameters, such as average grain size, crystallinity, strain, and crystal defects. X-ray diffraction peaks are produced by constructive interference of a monochromatic beam of X-rays scattered at specific angles from each set of lattice planes in a sample. The peak intensities are determined by the distribution of atoms within the lattice. Consequently, the X-ray diffraction pattern is the fingerprint of periodic atomic arrangements in a given material. This review summarizes the scientific trends associated with the rapid development of the technique of X-ray diffraction over the past five years pertaining to the fields of pharmaceuticals, forensic science, geological applications, microelectronics, and glass manufacturing, as well as in corrosion analysis.
X 射线衍射(XRD)是一种强大的、用于对晶体材料进行特征分析的非破坏性技术。它可以提供有关结构、相、优先晶体取向(织构)和其他结构参数(如平均晶粒尺寸、结晶度、应变和晶体缺陷)的信息。X 射线衍射峰是由样品中每个晶格平面的散射单束 X 射线的相干干涉产生的。峰强度由晶格内原子的分布决定。因此,X 射线衍射图案是给定材料中周期性原子排列的指纹。这篇综述总结了过去五年与制药、法医学、地质应用、微电子学和玻璃制造以及腐蚀分析等领域相关的 X 射线衍射技术快速发展的科学趋势。