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基于聚乳酸和榴莲皮纤维素的生物复合材料制备优化的响应面法

Response Surface Methodology for the Optimization of Preparation of Biocomposites Based on Poly(lactic acid) and Durian Peel Cellulose.

作者信息

Penjumras Patpen, Rahman Russly Abdul, Talib Rosnita A, Abdan Khalina

机构信息

Department of Process and Food Engineering, Faculty of Engineering, Universiti Putra Malaysia (UPM), 43400 Serdang, Selangor, Malaysia ; Department of Food Science and Technology, Maejo University, Phrae Campus, Phrae 54140, Thailand.

Department of Process and Food Engineering, Faculty of Engineering, Universiti Putra Malaysia (UPM), 43400 Serdang, Selangor, Malaysia ; Department of Food Technology, Faculty of Food Science and Technology, Universiti Putra Malaysia (UPM), 43400 Serdang, Selangor, Malaysia.

出版信息

ScientificWorldJournal. 2015;2015:293609. doi: 10.1155/2015/293609. Epub 2015 Jun 18.

Abstract

Response surface methodology was used to optimize preparation of biocomposites based on poly(lactic acid) and durian peel cellulose. The effects of cellulose loading, mixing temperature, and mixing time on tensile strength and impact strength were investigated. A central composite design was employed to determine the optimum preparation condition of the biocomposites to obtain the highest tensile strength and impact strength. A second-order polynomial model was developed for predicting the tensile strength and impact strength based on the composite design. It was found that composites were best fit by a quadratic regression model with high coefficient of determination (R (2)) value. The selected optimum condition was 35 wt.% cellulose loading at 165°C and 15 min of mixing, leading to a desirability of 94.6%. Under the optimum condition, the tensile strength and impact strength of the biocomposites were 46.207 MPa and 2.931 kJ/m(2), respectively.

摘要

采用响应面法优化基于聚乳酸和榴莲皮纤维素的生物复合材料的制备。研究了纤维素含量、混合温度和混合时间对拉伸强度和冲击强度的影响。采用中心复合设计来确定生物复合材料的最佳制备条件,以获得最高的拉伸强度和冲击强度。基于复合设计建立了用于预测拉伸强度和冲击强度的二阶多项式模型。结果发现,复合材料最适合具有高决定系数(R²)值的二次回归模型。选定的最佳条件为纤维素含量35 wt.%、混合温度165°C和混合时间15分钟,可取性为94.6%。在最佳条件下,生物复合材料的拉伸强度和冲击强度分别为46.207 MPa和2.931 kJ/m²。

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