Ahn Jin-Soo, Yi Young-Ah, Lee Yoon, Seo Deog-Gyu
Department of Dental Biomaterials Science, Dental Research Institute, School of Dentistry, Seoul National University, 101 Daehak-ro, Jongno-gu, Seoul, Republic of Korea.
Department of Dentistry, Inje University, Seoul Paik Hospital, Marunae-ro 9, Jung-gu, Seoul, Republic of Korea.
Biomed Res Int. 2015;2015:389234. doi: 10.1155/2015/389234. Epub 2015 Oct 11.
This study was conducted to evaluate the effects of different phosphate monomer-containing primers on the shear bond strength between yttria-tetragonal zirconia polycrystal (Y-TZP) ceramics and MDP-containing self-adhesive resin cement.
Y-TZP ceramic surfaces were ground flat with #600-grit SiC paper and divided into six groups (n = 10). They were treated as follows: untreated (control), Metal/Zirconia Primer, Z-PRIME Plus, air abrasion, Metal/Zirconia Primer with air abrasion, and Z-PRIME Plus with air abrasion. MDP-containing self-adhesive resin cement was applied to the surface-treated Y-TZP specimens. After thermocycling, a shear bond strength test was performed. The surfaces of the Y-TZP specimens were analyzed under a scanning electron microscope. The bond strength values were statistically analyzed using one-way analysis of variance and the Student-Newman-Keuls multiple comparison test (P < 0.05).
The Z-PRIME Plus treatment combined with air abrasion produced the highest bond strength, followed by Z-PRIME Plus application, Metal/Zirconia Primer combined with air abrasion, air abrasion alone, and, lastly, Metal/Zirconia Primer application. The control group yielded the lowest results (P < 0.05).
The application of MDP-containing primer resulted in increased bond strength between Y-TZP ceramics and MDP-containing self-adhesive resin cements.
本研究旨在评估不同含磷酸盐单体的底漆对氧化钇四方多晶(Y-TZP)陶瓷与含10-甲基丙烯酰氧癸基二氢磷酸酯(MDP)的自粘结树脂水门汀之间剪切粘结强度的影响。
用600目碳化硅砂纸将Y-TZP陶瓷表面打磨平整,分为六组(n = 10)。处理方式如下:未处理(对照组)、金属/氧化锆底漆、Z-PRIME Plus、空气喷砂、金属/氧化锆底漆联合空气喷砂、Z-PRIME Plus联合空气喷砂。将含MDP的自粘结树脂水门汀应用于表面处理后的Y-TZP试件。热循环后,进行剪切粘结强度测试。在扫描电子显微镜下分析Y-TZP试件的表面。粘结强度值采用单因素方差分析和Student-Newman-Keuls多重比较检验进行统计学分析(P < 0.05)。
Z-PRIME Plus处理联合空气喷砂产生的粘结强度最高,其次是单独应用Z-PRIME Plus、金属/氧化锆底漆联合空气喷砂、单独空气喷砂,最后是单独应用金属/氧化锆底漆。对照组的结果最低(P < 0.05)。
含MDP底漆的应用导致Y-TZP陶瓷与含MDP的自粘结树脂水门汀之间的粘结强度增加。