Orji Ndubuisi G, Itoh Hiroshi, Wang Chumei, Dixson Ronald G, Walecki Peter S, Schmidt Sebastian W, Irmer Bernd
Engineering Physics Division, National Institute of Standards and Technology, Gaithersburg, MD, United States.
National Institute of Advanced Industrial Science and Technology AIST Tsukuba Central Research Institute of Instrumentation Frontier Nanoscale MicroSpectroscopic Analysis Group, Tsukuba, Japan.
Ultramicroscopy. 2016 Mar;162:25-34. doi: 10.1016/j.ultramic.2015.12.003. Epub 2015 Dec 9.
In atomic force microscopy (AFM) metrology, the tip is a key source of uncertainty. Images taken with an AFM show a change in feature width and shape that depends on tip geometry. This geometric dilation is more pronounced when measuring features with high aspect ratios, and makes it difficult to obtain absolute dimensions. In order to accurately measure nanoscale features using an AFM, the tip dimensions should be known with a high degree of precision. We evaluate a new AFM tip characterizer, and apply it to critical dimension AFM (CD-AFM) tips used for high aspect ratio features. The characterizer is made up of comb-shaped lines and spaces, and includes a series of gratings that could be used as an integrated nanoscale length reference. We also demonstrate a simulation method that could be used to specify what range of tip sizes and shapes the characterizer can measure. Our experiments show that for non re-entrant features, the results obtained with this characterizer are consistent to 1nm with the results obtained by using widely accepted but slower methods that are common practice in CD-AFM metrology. A validation of the integrated length standard using displacement interferometry indicates a uniformity of better than 0.75%, suggesting that the sample could be used as highly accurate and SI traceable lateral scale for the whole evaluation process.
在原子力显微镜(AFM)计量学中,探针是不确定性的一个关键来源。用AFM拍摄的图像显示出特征宽度和形状的变化,这取决于探针的几何形状。当测量高纵横比的特征时,这种几何扩张更为明显,并且难以获得绝对尺寸。为了使用AFM精确测量纳米级特征,需要高精度地了解探针尺寸。我们评估了一种新型AFM探针表征仪,并将其应用于用于高纵横比特征的关键尺寸AFM(CD-AFM)探针。该表征仪由梳状线条和间距组成,并包括一系列可用作集成纳米级长度参考的光栅。我们还展示了一种模拟方法,可用于确定表征仪能够测量的探针尺寸和形状范围。我们的实验表明,对于非凹入特征,使用该表征仪获得的结果与通过使用CD-AFM计量学中常用的、被广泛接受但速度较慢的方法所获得的结果在1nm范围内一致。使用位移干涉测量法对集成长度标准进行的验证表明,均匀性优于0.75%,这表明该样品可在整个评估过程中用作高度精确且可溯源至国际单位制的横向尺度。