Stawarczyk Bogna, Frevert Kathrin, Ender Andreas, Roos Malgorzata, Sener Beatrice, Wimmer Timea
Department of Prosthodontics, Dental School, Ludwig-Maximilians-University of Munich, Germany.
Department of Prosthodontics, Dental School, Ludwig-Maximilians-University of Munich, Germany.
J Mech Behav Biomed Mater. 2016 Jun;59:128-138. doi: 10.1016/j.jmbbm.2015.11.040. Epub 2015 Dec 23.
To test the mechanical and optical properties of monolithic zirconia in comparison to conventional zirconia.
Specimens were prepared from: monolithic zirconia: Zenostar (ZS), DD Bio ZX(2) hochtransluzent (DD), Ceramill Zolid (CZ), InCoris TZI (IC) and a conventional zirconia Ceramill ZI (CZI). Contrast ratio (N=75/n=15) was measured according to ISO 2471:2008. Grain sizes (N=75/n=15) were investigated with scanning electron microscope. Four-point flexural strength (N=225/n=15/zirconia and aging regime) was measured initially, after aging in autoclave or chewing simulator (ISO 13356:2008). Two-body wear of polished and glazed/veneered specimens (N=108/n=12) was analyzed in a chewing simulator using human teeth as antagonists. Data were analyzed using 2-/1-way ANOVA with post-hoc Scheffé, Kruskal-Wallis-H, Mann-Whitney-U, Spearman-Rho, Weibull statistics and linear mixed models (p<0.05).
The lowest contrast ratio values were found for ZS and IC and CZ. IC showed the largest grain size followed by DD and CZI. The smallest grain size was observed for ZS followed by CZ. There was no correlation between grain size and contrast ratio. The aging regime showed no impact on flexural strength. All non-aged and autoclave-aged specimens showed lower flexural strengths than the control group CZI. Within groups aged in chewing simulator, ZS showed significantly lower flexural strength than CZI. CZI showed higher material and antagonist wear than monolithic polished and glazed groups. Glazed specimens showed higher material and antagonist loss compared to polished ones. There was no correlation between roughness and wear.
Monolithic zirconia showed higher optical, but lower mechanical properties than conventional zirconia.
测试整体式氧化锆与传统氧化锆相比的机械性能和光学性能。
制备以下材料的样本:整体式氧化锆:Zenostar(ZS)、DD Bio ZX(2) hochtransluzent(DD)、Ceramill Zolid(CZ)、InCoris TZI(IC)以及传统氧化锆Ceramill ZI(CZI)。根据ISO 2471:2008测量对比度(N = 75/n = 15)。用扫描电子显微镜研究晶粒尺寸(N = 75/n = 15)。最初测量四点弯曲强度(N = 225/n = 15/氧化锆及老化状态),之后在高压灭菌器或咀嚼模拟器中老化后测量(ISO 13356:2008)。在咀嚼模拟器中使用人牙作为对抗物分析抛光和釉面/贴面样本的两体磨损(N = 108/n = 12)。使用双因素/单因素方差分析以及事后Scheffé检验、Kruskal-Wallis-H检验、Mann-Whitney-U检验、Spearman-Rho检验、威布尔统计和线性混合模型分析数据(p<0.05)。
ZS、IC和CZ的对比度值最低。IC的晶粒尺寸最大,其次是DD和CZI。观察到ZS的晶粒尺寸最小,其次是CZ。晶粒尺寸与对比度之间无相关性。老化状态对弯曲强度无影响。所有未老化和高压灭菌老化的样本的弯曲强度均低于对照组CZI。在咀嚼模拟器中老化的组内,ZS的弯曲强度显著低于CZI。CZI的材料磨损和对抗物磨损高于整体式抛光和釉面组。与抛光样本相比,釉面样本的材料损失和对抗物损失更高。粗糙度与磨损之间无相关性。
整体式氧化锆显示出比传统氧化锆更高的光学性能,但机械性能较低。