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不同百分比的微羟基磷灰石对树脂改性玻璃离子体和锆聚体微硬度的影响。

Effects of Different Percentages of Microhydroxyapatite on Microhardness of Resin-modified Glass-ionomer and Zirconomer.

作者信息

Sharafeddin Farahnaz, Shoale Soodabe, Kowkabi Mahsa

机构信息

Professor of Dept. of Operative Dentistry, Biomaterial Research Center, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.

Postgraduate Student, Dept. of Operative Dentistry, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.

出版信息

J Clin Exp Dent. 2017 Jun 1;9(6):e805-e811. doi: 10.4317/jced.53668. eCollection 2017 Jun.

Abstract

BACKGROUND

Hydroxyapatite (HA) is the main mineral component of the tooth structure, which exhibits considerable biological behavior and its incorporation might improve microhardness of dental materials. Microhardness of restorative materials, like glass-ionomer, is critical for the clinical longevity of restorations. The aim of this study was to evaluate the microhardness of two glass-ionomers types by incorporating different percentages of microhydroxyapatite.

MATERIAL AND METHODS

In this study, 80 disc-shaped experimental specimens (6 mm in diameter, 2 mm in height) were prepared in 8 groups, including resin-modified glass-ionomer (RMGI, GC, Gold Label, Japan), zirconia-reinforced glass-ionomer (Zirconomer, Shofu, Kyoto, Japan), and their mixture with 0, 5, 15 and 25 wt% of microhydroxyapatite (Sigma-Aldrich, Germany). All the specimens were stored in deionized water at 37ºC for 24 hours. Then Vickers microhardness test was carried out on the both sides of specimens and data were analyzed using two-way ANOVA and paired t-test (<0.05).

RESULTS

Microhardness of Zirconomer and RMGI increased significantly due to adding 5 and 15 wt% of micrhydrox-yapatite (<0.001). The highest Vickers hardness number (VHN) was recorded in the RMGI group with 5 wt% of microhydroxyapatite. In addition, in all the study groups RMGI exhibited higher microhardness values than Zirconomer (<0.001). However, microhardness values decreased significantly after adding 25 wt% of microhydroxyapatite to Zirconomer (<0.001). Similarly, VHN decreased in RMGI groups containing 25 wt% of HA compared to control groups (without HA) (<0.001).

CONCLUSIONS

Incorporation of 5 and 15 wt% of microhydroxyapatite to RMGI and Zirconomer improved microhardness, while adding 25 wt% of HA decreased hardness with both experimental materials compared to the control groups (without HA). Microhardness, Resin-modified glass-ionomer, Zirconia-reinforced glass ionomer, Microhydroxyapatite.

摘要

背景

羟基磷灰石(HA)是牙齿结构的主要矿物质成分,具有显著的生物学特性,将其加入牙科材料中可能会提高材料的显微硬度。修复材料(如玻璃离子水门汀)的显微硬度对修复体的临床使用寿命至关重要。本研究的目的是通过加入不同百分比的微羟基磷灰石来评估两种玻璃离子水门汀的显微硬度。

材料与方法

在本研究中,制备了8组共80个圆盘形实验样本(直径6mm,高2mm),包括树脂改性玻璃离子水门汀(RMGI,GC,金标,日本)、氧化锆增强玻璃离子水门汀(Zirconomer,松风,京都,日本),以及它们与0、5、15和25wt%微羟基磷灰石(西格玛奥德里奇,德国)的混合物。所有样本在37℃的去离子水中储存24小时。然后在样本的两面进行维氏显微硬度测试,并使用双向方差分析和配对t检验(<0.05)对数据进行分析。

结果

由于加入5wt%和15wt%的微羟基磷灰石,Zirconomer和RMGI的显微硬度显著增加(<0.001)。在含5wt%微羟基磷灰石的RMGI组中记录到最高的维氏硬度值(VHN)。此外,在所有研究组中,RMGI的显微硬度值均高于Zirconomer(<0.001)。然而,在Zirconomer中加入25wt%微羟基磷灰石后,显微硬度值显著降低(<0.001)。同样,与对照组(不含HA)相比,含25wt%HA的RMGI组的VHN降低(<0.001)。

结论

向RMGI和Zirconomer中加入5wt%和15wt%的微羟基磷灰石可提高显微硬度,而与对照组(不含HA)相比,向两种实验材料中加入25wt%的HA均会降低硬度。显微硬度、树脂改性玻璃离子水门汀、氧化锆增强玻璃离子水门汀、微羟基磷灰石。

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