Oceanography Section, Science Research Center, Kochi University, Akebono-cho 2-5-1, Kochi City, Kochi 780-8520, Japan.
Oceanography Section, Science Research Center, Kochi University, Akebono-cho 2-5-1, Kochi City, Kochi 780-8520, Japan; Research Laboratory of Hydrothermal Chemistry, Faculty of Science, Kochi, University, Akebono-cho 2-5-1, Kochi City, Kochi 780-8520, Japan.
Food Chem. 2016 Nov 1;210:311-6. doi: 10.1016/j.foodchem.2016.04.121. Epub 2016 Apr 26.
Microwave-assisted hydrothermal extraction was applied for production of sulfated polysaccharides from Ulva spp. and Monostroma latissimum. The maximum ulvan yields attained 40.4±3.2% (Ulva meridionalis) and 36.5±3.1% (Ulva ohnoi) within 4min of come-up time and 10min of extraction time at 160°C, respectively. The rhamnan sulfate yield from M. latissimum further attained 53.1±7.2% at 140°C. The sulfated polysaccharides were easily recovered from the extract by simple ethanol precipitation. In addition, molecular weights and viscosity of the extracted polysaccharides could be controlled by varying the extraction temperature. Dielectric measurement revealed that ionic conduction was the important parameter that affect the microwave susceptibility of algae-water mixture. The sulfated polysaccharides extracts are expected as potential feedstock for medical and food applications.
微波辅助水热提取法被应用于从石莼属和鹅肠菜属中提取硫酸多糖。在 160°C 下,提取时间为 4 分钟和 10 分钟时,最大的岩藻聚糖产率分别达到 40.4±3.2%(南方石莼)和 36.5±3.1%(孔石莼)。140°C 时,从鹅肠菜属中提取的硫酸鼠李聚糖的产率进一步达到 53.1±7.2%。通过简单的乙醇沉淀可以从提取物中轻松回收硫酸多糖。此外,通过改变提取温度可以控制提取多糖的分子量和粘度。介电测量表明,离子传导是影响海藻-水混合物微波敏感性的重要参数。硫酸多糖提取物有望成为医学和食品应用的潜在原料。