Villefort Regina Furbino, Amaral Marina, Pereira Gabriel Kalil Rocha, Campos Tiago Moreira Bastos, Zhang Yu, Bottino Marco Antonio, Valandro Luiz Felipe, de Melo Renata Marques
PhD Graduate Program in Restorative Dentistry, Prosthetic Dentistry Unit, School of Dentistry, São Paulo State University, Av. Eng Franscisco José Longo, 777, São José dos Campos, SP 12245-000, Brazil.
PhD Graduate Program in Oral Science, Prosthetic Dentistry Unit, Federal University of Santa Maria, R. Floriano Peixoto, 1184, Santa Maria, RS 97015-372, Brazil.
Dent Mater. 2017 Apr;33(4):e155-e164. doi: 10.1016/j.dental.2016.12.010. Epub 2017 Jan 21.
This study evaluated the effects of two grading techniques of zirconia material on the fatigue limit of full-contour 3-unit fixed dental prostheses (FDPs).
Presintered blocks of 3Y-TZP were milled to obtain sixty-nine 3-unit FDPs, which were divided into three groups (n=23). The control group (CTL) was sintered and glazed following manufacturer's instructions. In the two experimental groups presintered FDPs received a surface silica/glass infiltration treatment before the sintering process. Silica sol-gel group (SSG) was graded by the sol-gel processing route, while the glass-zirconia-glass group (GZG) was graded by an enameling technique. Graded groups did not receive a glaze layer after sintering. All FDPs were then luted with a dual-curing resin cement on composite abutments, embedded in polyurethane and stored in water for five days. The initial load of the fatigue test was calculated based on the results of the monotonic testing applied on three specimens of each group. To determine the fatigue limit, 20 samples of each group were subjected to staircase testing (100,000 cycles/5Hz).
The fatigue limits (in Newtons) were CTL=1607.27, SSG=1824.31, and GZG=2006.57, and the Dixon and Mood test indicated statistically significant differences among groups (95% confidence interval) (GZG > SSG > CTL).
The infiltration of silica and glass on bulk zirconia, by two different grading methods, increased the fatigue limits of monolithic zirconia FDPs.
本研究评估了两种氧化锆材料分级技术对全冠3单位固定义齿(FDP)疲劳极限的影响。
将预烧结的3Y-TZP块体进行研磨,以获得69个3单位FDP,将其分为三组(n = 23)。对照组(CTL)按照制造商的说明进行烧结和上釉。在两个实验组中,预烧结的FDP在烧结过程之前接受表面二氧化硅/玻璃渗透处理。硅溶胶-凝胶组(SSG)通过溶胶-凝胶工艺路线进行分级,而玻璃-氧化锆-玻璃组(GZG)通过搪瓷技术进行分级。分级后的组在烧结后不接受釉层。然后,所有FDP用双固化树脂粘结剂粘结在复合基台上,嵌入聚氨酯中并在水中储存5天。根据对每组三个样本进行的单调测试结果计算疲劳试验的初始载荷。为了确定疲劳极限,对每组20个样本进行阶梯测试(100,000次循环/5Hz)。
疲劳极限(以牛顿为单位)分别为CTL = 1607.27,SSG = 1824.31和GZG = 2006.57,迪克森和穆德检验表明各组之间存在统计学显著差异(95%置信区间)(GZG > SSG > CTL)。
通过两种不同的分级方法,在块状氧化锆上渗透二氧化硅和玻璃,提高了整体式氧化锆FDP的疲劳极限。