Denisyuk Andrey, Hrnčíř Tomáš, Vincenc Oboňa Jozef, Petrenec Martin, Michalička Jan
1TESCAN ORSAY HOLDING,Libušina třída 21,62300 Brno,Czech Republic.
2TESCAN Brno,Libušina třída 1,62300 Brno,Czech Republic.
Microsc Microanal. 2017 Jun;23(3):484-490. doi: 10.1017/S1431927617000241. Epub 2017 Mar 20.
We report on the mitigation of curtaining artifacts during transmission electron microscopy (TEM) lamella preparation by means of a modified ion beam milling approach, which involves altering the incident angle of the Ga ions by rocking of the sample on a special stage. We applied this technique to TEM sample preparation of a state-of-the-art integrated circuit based on a 14-nm technology node. Site-specific lamellae with a thickness <15 nm were prepared by top-down Ga focused ion beam polishing through upper metal contacts. The lamellae were analyzed by means of high-resolution TEM, which showed a clear transistor structure and confirmed minimal curtaining artifacts. The results are compared with a standard inverted thinning preparation technique.
我们报告了通过一种改进的离子束铣削方法来减轻透射电子显微镜(TEM)薄片制备过程中的幕帘状伪像,该方法涉及通过在特殊平台上摇动样品来改变Ga离子的入射角。我们将此技术应用于基于14纳米技术节点的先进集成电路的TEM样品制备。通过自上而下的Ga聚焦离子束抛光穿过上层金属接触,制备了厚度<15纳米的特定位置薄片。通过高分辨率TEM对薄片进行分析,结果显示出清晰的晶体管结构,并证实了幕帘状伪像极少。将结果与标准的反向减薄制备技术进行了比较。