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硝酸-氢氟酸对氧化锆表面处理对树脂水门汀剪切粘结强度的影响。

Effect of zirconia surface treatment using nitric acid-hydrofluoric acid on the shear bond strengths of resin cements.

作者信息

Cho Jin Hyung, Kim Sun Jai, Shim June Sung, Lee Keun-Woo

机构信息

Department of Prosthodontics, Graduate School, Yonsei University, Seoul, Republic of Korea.

出版信息

J Adv Prosthodont. 2017 Apr;9(2):77-84. doi: 10.4047/jap.2017.9.2.77. Epub 2017 Apr 6.

DOI:10.4047/jap.2017.9.2.77
PMID:28435615
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC5397592/
Abstract

PURPOSE

The aim of this study was to compare the surface roughness of zirconia when using Zircos E etching system (ZSAT), applying a nitric acid-hydrofluoric acid compound as a pretreatment agent, and also to compare the shear bonding strength according to different resin cements.

MATERIALS AND METHODS

ZSAT, air abrasion, and tribochemical silicacoating were applied on prepared 120 zirconia specimens (10 mm in diameter, 7 mm in height) using CAD/CAM. Each 12 specimens with 4 different resin cements (Panavia F 2.0, Rely X Unicem, Superbond C&B, and Hot bond) were applied to test interfacial bond strength. The statistical analysis was performed using SAS 9.1 (SAS Institute Inc., Cary, NC, USA). The results are as follows: after application of the ZSAT on the zirconia specimens, surface roughness value after 2-hour etching was higher than those after 1- and 3-hour etching on SEM images.

RESULTS

For Superbond C&B and Rely X Unicem, the specimens treated with ZSAT showed higher shear bond strength values than those treated with air abrasion and tribochemical silicacoating system. Regarding the failure mode of interface over cement and zirconia surface, Rely X Unicem and Hot bond showed cohesive failures and Panavia F 2.0 and Superbond C&B showed mixed failures.

CONCLUSION

Zircos E etching system in zirconia restoration could increase its shear bond strength. However, its long term success rate and clinical application should be further evaluated.

摘要

目的

本研究旨在比较使用Zircos E蚀刻系统（ZSAT）时氧化锆的表面粗糙度，该系统采用硝酸 - 氢氟酸化合物作为预处理剂，同时还比较不同树脂水门汀的剪切粘结强度。

材料与方法

使用CAD/CAM技术，对制备好的120个氧化锆标本（直径10毫米，高7毫米）分别应用ZSAT、空气喷砂和摩擦化学硅涂层处理。每种处理后的12个标本分别与4种不同的树脂水门汀（Panavia F 2.0、Rely X Unicem、Superbond C&B和Hot bond）结合，以测试界面粘结强度。使用SAS 9.1（美国北卡罗来纳州卡里市SAS研究所）进行统计分析。结果如下：在氧化锆标本上应用ZSAT后，扫描电子显微镜图像显示，蚀刻2小时后的表面粗糙度值高于蚀刻1小时和3小时后的。

结果

对于Superbond C&B和Rely X Unicem，经ZSAT处理的标本显示出比经空气喷砂和摩擦化学硅涂层系统处理的标本更高的剪切粘结强度值。关于水门汀与氧化锆表面之间界面的失效模式，Rely X Unicem和Hot bond表现为内聚性失效，而Panavia F 2.0和Superbond C&B表现为混合性失效。

结论

氧化锆修复中使用的Zircos E蚀刻系统可提高其剪切粘结强度。然而，其长期成功率和临床应用仍需进一步评估。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/d6cf8c8e17a9/jap-9-77-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/b92366dbf4b2/jap-9-77-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/894a7920fe2a/jap-9-77-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/42fcffad4b29/jap-9-77-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/cd4f88c22234/jap-9-77-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/c526215119dc/jap-9-77-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/321f0d828738/jap-9-77-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/a3a18a86dee2/jap-9-77-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/f1b06398e024/jap-9-77-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/d6cf8c8e17a9/jap-9-77-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/b92366dbf4b2/jap-9-77-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/894a7920fe2a/jap-9-77-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/42fcffad4b29/jap-9-77-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/cd4f88c22234/jap-9-77-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/c526215119dc/jap-9-77-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/321f0d828738/jap-9-77-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/a3a18a86dee2/jap-9-77-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/f1b06398e024/jap-9-77-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2662/5397592/d6cf8c8e17a9/jap-9-77-g009.jpg

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