Zhao Yarong, Wang Qiongshan, Huang Jianxiang, Ma Liyan, Chen Zhihui, Wang Fuhua
a Public Monitoring Center for Agro-product of Guangdong Academy of Agricultural Sciences , Guangzhou , China.
b College of Food Science and Nutritional Engineering , China Agricultural University , Beijing , China.
Food Addit Contam Part B Surveill. 2018 Mar;11(1):9-14. doi: 10.1080/19393210.2017.1388295. Epub 2017 Nov 8.
Wheat is an important cereal but it is often contaminated with mycotoxins. The natural occurrence of aflatoxin B (AFB) and sterigmatocystin (STC) was determined in 178 food samples (32 wheat samples and 146 wheat products) purchased from Chinese supermarkets. The methodology was validated, the wheat and wheat products samples were treated with a modified QuEChERS (quick, easy, cheap, effective, rugged, and safe) and quantified by liquid chromatography-tandem mass spectrometry (LC-MS/MS). From these samples 18.8% of wheat and 8.2% of cracker samples were contaminated with AFB. Mean levels were 0.06 µg/kg and 0.05µg/kg, respectively. There was no AFB contamination in white bread or whole meal bread. Meanwhile 53.1% of wheat, 59.2% of crackers, 20.8% of white bread and 16% of whole meal bread samples were contaminated with STC. The mean levels were 0.07, 0.79, 0.12 and 0.12 µg/kg respectively. Although the levels were low, this demonstrates the need for more comprehensive surveys for these two mycotoxins in wheat and wheat products from China.
小麦是一种重要的谷物,但它经常被霉菌毒素污染。对从中国超市购买的178份食品样本(32份小麦样本和146份小麦制品)中黄曲霉毒素B(AFB)和柄曲霉素(STC)的天然存在情况进行了测定。该方法经过验证,小麦和小麦制品样本采用改良的QuEChERS(快速、简便、廉价、有效、耐用且安全)方法处理,并通过液相色谱 - 串联质谱法(LC - MS/MS)进行定量。在这些样本中,18.8%的小麦和8.2%的饼干样本被AFB污染。平均含量分别为0.06微克/千克和0.05微克/千克。白面包或全麦面包中未检测到AFB污染。同时,53.1%的小麦、59.2%的饼干、20.8%的白面包和16%的全麦面包样本被STC污染。平均含量分别为0.07、0.79、0.12和0.12微克/千克。尽管含量较低,但这表明有必要对中国小麦和小麦制品中的这两种霉菌毒素进行更全面的调查。