Sanmugam Anandhavelu, Vikraman Dhanasekaran, Park Hui Joon, Kim Hyun-Seok
Department of Chemistry (S&H), Vel Tech Multitech Dr.Rangarajan Dr.Sakunthala Engineering College, Chennai 600062, India.
Division of Electronics and Electrical Engineering, Dongguk University-Seoul, Seoul 04620, Korea.
Nanomaterials (Basel). 2017 Nov 2;7(11):363. doi: 10.3390/nano7110363.
Novel chitosan-ZnO-graphene oxide hybrid composites were prepared using a one-pot chemical strategy, and their dye adsorption characteristics and antibacterial activity were demonstrated. The prepared chitosan and the hybrids such as chitosan-ZnO and chitosan-ZnO-graphene oxide were characterized by UV-Vis absorption spectroscopy, X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, and transmission electron microscopy. The thermal and mechanical properties indicate a significant improvement over chitosan in the hybrid composites. Dye adsorption experiments were carried out using methylene blue and chromium complex as model pollutants with the function of dye concentration. The antibacterial properties of chitosan and the hybrids were tested against Gram-positive and Gram-negative bacterial species, which revealed minimum inhibitory concentrations (MICs) of 0.1 µg/mL.
采用一锅法化学策略制备了新型壳聚糖-氧化锌-氧化石墨烯杂化复合材料,并对其染料吸附特性和抗菌活性进行了表征。通过紫外可见吸收光谱、X射线衍射、傅里叶变换红外光谱、扫描电子显微镜和透射电子显微镜对制备的壳聚糖以及壳聚糖-氧化锌和壳聚糖-氧化锌-氧化石墨烯等杂化物进行了表征。热性能和力学性能表明,杂化复合材料相对于壳聚糖有显著改善。以亚甲基蓝和铬络合物为模型污染物,研究了染料浓度对染料吸附实验的影响。测试了壳聚糖及其杂化物对革兰氏阳性和革兰氏阴性细菌的抗菌性能,结果显示最低抑菌浓度(MICs)为0.1μg/mL。