Angle Orthod. 2018 Mar;88(2):221-226. doi: 10.2319/070917-455.1. Epub 2017 Nov 15.
To investigate the shear bond strength (SBS) of orthodontic metal brackets applied to different types of ceramic surfaces treated with different etching procedures and bonding agents.
Monolithic CAD/CAM ceramic specimens (N = 120; n = 40 each group) of feldspathic ceramic Vita Mark II, resin nanoceramic Lava Ultimate, and hybrid ceramic Vita Enamic were fabricated (14 × 12 × 3 mm). Ceramic specimens were separated into four subgroups (n = 10) according to type of surface treatment and bonding onto the ceramic surface. Within each group, four subgroups were prepared by phosphoric acid, hydrofluoric acid, Transbond XT primer, and Clearfill Ceramic primer. Mandibular central incisor metal brackets were bonded with light-cure composite. The SBS data were analyzed using three-way analysis of variance (ANOVA) and Tukey HSD tests.
The highest SBS was found in the Vita Enamic group, which is a hybrid ceramic, etched with hydrofluoric acid and applied Transbond XT Adhesive primer (7.28 ± 2.49 MPa). The lowest SBS was found in the Lava Ultimate group, which is a resin nano-ceramic etched with hydrofluoric acid and applied Clearfill ceramic primer (2.20 ± 1.21 MPa).
CAD/CAM material types and bonding procedures affected bond strength ( P < .05), but the etching procedure did not ( P > .05). The use of Transbond XT as a primer bonding agent resulted in higher SBS.
研究不同类型的陶瓷表面经不同酸蚀处理和黏接剂处理后,正畸金属托槽的剪切黏结强度(SBS)。
制作了整块 CAD/CAM 陶瓷标本(N = 120;n = 40 每组),包括长石陶瓷 Vita Mark II、树脂纳米陶瓷 Lava Ultimate 和混合陶瓷 Vita Enamic(14×12×3mm)。根据表面处理和黏接剂在陶瓷表面上的应用,将陶瓷标本分为四组(n = 10)。在每组中,通过磷酸、氢氟酸、Transbond XT 底漆和 Clearfill Ceramic 底漆制备了四个亚组。用光固化复合树脂黏接下颌中切牙金属托槽。使用三因素方差分析(ANOVA)和 Tukey HSD 检验对 SBS 数据进行分析。
SBS 最高的是混合陶瓷 Vita Enamic,经氢氟酸酸蚀并用 Transbond XT 黏接剂处理(7.28±2.49MPa)。SBS 最低的是树脂纳米陶瓷 Lava Ultimate,经氢氟酸酸蚀并用 Clearfill Ceramic 底漆处理(2.20±1.21MPa)。
CAD/CAM 材料类型和黏接程序影响黏结强度(P<.05),但酸蚀程序不影响(P>.05)。使用 Transbond XT 作为底漆黏接剂可获得更高的 SBS。